Plugging agent for drilling fluid and preparation method thereof
A lost circulation agent and drilling fluid technology, which is applied in the field of lost circulation blocking agent for drilling fluid and its preparation, and can solve the problems of resistance to water dilution, poor fluidity, and decreased retention capacity.
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Embodiment 1
[0044]Dissolve 25g of polysulfone in methylene chloride, then add a mixture of 79g of CYD-128 epoxy resin and 3.8g of benzyl alcohol, stir evenly to form a dispersed phase; use 1.0% sodium dodecylbenzenesulfonate aqueous solution as the continuous phase, The above-mentioned dispersed phase is added dropwise into the continuous phase while stirring at a high speed at a speed of 2600 r / min. After the dropwise addition, react in a constant temperature water bath at 40° C. for 5.5 hours while stirring at a low speed at 600 r / min. After the complete volatilization reaction of dichloromethane is completed, wash with ethanol and then with deionized water, and finally perform suction filtration and dry in an oven at 65° C. for 12 hours to obtain the microcapsule modifier.
[0045] 200g of straight-run asphalt with a softening point of 46.8°C, 21.2g of Span-80 and 250g of water were emulsified with a high shear machine, and 27.6g of cocoyl 1,3-propylenediamine and 3.6g of 4, The 4-dia...
Embodiment 2
[0047] Dissolve 32.6g of polyethersulfone in dichloromethane, then add a mixture of 148.4g of CYD-128 epoxy resin and 8.5g of benzyl alcohol, stir well to form a dispersed phase; use 1.5% sodium dodecylbenzenesulfonate aqueous solution as Continuous phase, the above-mentioned dispersed phase is added dropwise into the continuous phase, and high-speed stirring is carried out at the same time, and the rotation speed is 2200r / min. After the dropwise addition, react in a constant temperature water bath at 45° C. for 6 hours while stirring at a low speed at 500 r / min. After the complete volatilization reaction of dichloromethane is completed, wash with ethanol and then with deionized water, and finally perform suction filtration and dry in an oven at 60° C. for 15 hours to obtain the microcapsule modifier.
[0048] 200g of oxidized asphalt with a softening point of 63.5°C, 16.8g of polyoxyethylene stearate and 280g of water were shear emulsified with a high shear machine, and 35.5g...
Embodiment 3
[0050] Dissolve 45.5g polysulfone in dichloromethane, then add the mixture of 121.6g E-44 epoxy resin and 5.8g benzyl alcohol, stir well to form a dispersed phase; use 1.0% sodium dodecylbenzenesulfonate aqueous solution as continuous Phase, the above-mentioned dispersed phase was added dropwise into the continuous phase, while stirring at a high speed, the rotation speed was 2000r / min. After the dropwise addition, react in a constant temperature water bath at 35° C. for 7 hours while stirring at a low speed at 650 r / min. After the complete volatilization reaction of dichloromethane is completed, wash with ethanol and then with deionized water, and finally perform suction filtration and dry in an oven at 70° C. for 16 hours to obtain the microcapsule modifier.
[0051] 200g of oxidized pitch with a softening point of 70.2°C, 31.5g of Span-85 and 320g of water were emulsified with a high shear machine, and 38.8g of hexadecyldimethyl tertiary amine and 4.0g of 4,4-bis Continue ...
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