A super explosion-proof and impact-resistant composite coating and its preparation method
A composite coating and impact-resistant technology, applied in the field of coatings, can solve the problems of difficult dispersion of graphene, poor dispersion of fillers, unfavorable coating film strength and modulus, etc., and achieve the effect of avoiding expensive prices and excellent tensile strength
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Embodiment 1
[0047] 1.1) Flexible coating material A component and B components
[0048] A Component:
[0049] MDI50 59kg;
[0050] Polyteylvaramid etheriol (PTMG-1000) 41kg;
[0051] B Component:
[0052] Dimethylthio-diomylamine (DMTDA) 20kg;
[0053] N, N'-bimensional cyclohexane (Jefflink754) 20 kg;
[0054] Polyether amine CAT-5000 10kg;
[0055] Polyether amine CAD2000 42.1kg;
[0056] KH550 silane coupling agent 0.5kg;
[0057] Active sulfate calcium sulfate must be NP-M02 5kg;
[0058] Special carbon black pulp 2.3kg;
[0059] BYK-023 0.05kg;
[0060] BYK-410 0.05kg.
[0061] 1.2) Preparation of a component
[0062] In a reaction bottle equipped with 59kg MDI-50, a nitrogen gas is passed into a nitrogen, stirred, heating to 50 ° C, divided into two batches of 41 kg of PTMG-1000 after the preheating, 10 minutes of two batches of time, after it is completed The temperature was raised to 75 ° C to 95 ° C, and the reaction was continued for 3 hours, the sampling determination of the -NCO e...
Embodiment 2
[0103] The preparation of the A component, the B component, the C component, the D component preparation step and the composite coating is repeated, and only the A component, the B component, the C component, and the amount of material Ingoin Other as in Example 1. Raw material distribution range adjustment:
[0104] 1.1) Flexible coating material A component and B components
[0105] A component: MDI50 56.5kg, polytetrahydrofuran (PTMG-1000) 43.5 kg.
[0106] Component: dimethylthiomethaliamine (DMTDA) 20 kg, N, N'-bispentyl cyclohexane (Jefflink754) 18.5 kg; polyether amine CAT-5000 15 kg, polyether amine CAD2000 38.6 kg; KH550 silane coupling agent 0.5kg; active whisker silicon (GX-SiO 2 5kg; special carbon black pulp 2.3kg; BYK-023 0.05 kg; BYK-410 0.05kg.
[0107] 1.2) Preparation of a component
[0108] In a reaction bottle containing 56.5 kg of MDI-50, nitrogen, start stirring, warmed to 50 ° C, divided into two batchs of 43.5 kg of PTMG-1000 after preheating, two batches o...
Embodiment 3
[0126] The preparation of the A component, the B component, the C component, the D component preparation step and the composite coating is repeated, and only the A component, the B component, the C component, and the amount of material Ingoin Other as in Example 1. Raw material distribution range adjustment:
[0127] 1.1) Flexible coating material A component and B components
[0128] A component: MDI-100 66.2kg, polytegant hydrogenfuranyl nanol (PTMG-1000) 33.8 kg.
[0129] Component: N, N 'Dialkylphenylenediamine (UniLink 4100) 35 kg, N, N'-bispentylcyclohexane (Jefflink754) 15 kg; polyether amine CAT-5000 2kg, polyether amine CAD2000 43.4kg; KH550 silane coupling agent 0.5 kg; activated sulfate (NP-M02) 3kg; special carbon black pulp 1kg; BYK-023 0.05 kg; BYK-410 0.05 kg.
[0130] 1.2) Preparation of a component
[0131] In a reaction bottle equipped with 66.2 kg of MDI-100, a nitrogen gas is passed into nitrogen, start stirring, warmed to 50 ° C, divided into two batchs of 33....
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