Polycrystalline resin diamond abrasive and preparation method thereof
A polycrystalline diamond and diamond technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of limited use range, shortened service life, and poor processing quality of diamond abrasives, and achieve lighter color and increased crystal transparency , The effect of improving thermal stability
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[0022] A preparation method of polycrystalline resin diamond abrasive, specifically, the uniform mixed powder of polycrystalline diamond abrasive, metal and alloy is synthesized by high temperature and high pressure method, and the metal and alloy account for 5%-16% of the weight of the mixed powder; The metal is at least one of copper, aluminum and zinc, and the alloy is at least one of copper-zinc alloy and copper-aluminum alloy. The polycrystalline diamond abrasive of the present application is a commercially available polycrystalline diamond abrasive synthesized by a conventional high temperature and high pressure method.
[0023] Specifically, the cleaned polycrystalline diamond abrasive, metal and alloy powder are evenly mixed and put into a metal cup. Metal cups are made of stainless steel, zirconium, niobium, molybdenum or tantalum. After that, pyrophyllite blocks are put into it and then synthesized in a six-sided top press under high temperature and high pressure. ...
Embodiment 1
[0028] A certain particle size of polycrystalline diamond abrasive synthesized by a conventional high temperature and high pressure method is selected as a raw material, and 5.5% of zinc, 3% of copper, and 1.5% of Cu85Al15 are added. After mixing evenly, put it into a molybdenum cup, and then put it into a synthesis block and put it into a six-sided top press for high-temperature and high-pressure synthesis.
[0029] Boost the pressure to the high pressure of the hydraulic system of the press to 100MPa within 50 seconds. After the internal synthetic pressure reaches 6300MPa, keep the pressure for 14 minutes.
[0030] Start heating after boosting the pressure for 80 seconds, the heating temperature is 1350-1450 degrees Celsius, and the heating time is 10 minutes.
Embodiment 2
[0032] The polycrystalline diamond abrasive 60 / 80-400 / 500 mesh mixture synthesized by the conventional high temperature and high pressure method is selected as the raw material, and 2.5% of aluminum, 1% of copper, 2.5% of Cu85Al15, and 4% of Cu60Zn40 are added to the molybdenum cup after mixing evenly.
[0033] It takes 60 seconds to increase the pressure to the high pressure of the hydraulic system of the press to 100MPa. After the internal synthetic pressure reaches 6300MPa, keep the pressure for 12 minutes. After 70 seconds of increasing the pressure, start heating. Heating temperature to 1350-1450 degrees Celsius, heating time 8 minutes.
[0034] According to the synthetic method of embodiment 1, select polycrystalline diamond abrasive of different grain sizes as the TI and TTI / TI performance of the polycrystalline resin diamond abrasive produced by raw material and commercially available single crystal resin diamond abrasive and commercially available polycrystalline res...
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