Nickel-chromium alloy sputtering target materials and hot isostatic pressing preparation method thereof

A hot isostatic pressing, nickel-chromium alloy technology, applied in sputtering coating, metal material coating process, vacuum evaporation coating, etc. The target material does not meet the sputtering requirements and other problems, so as to achieve the effect of small grain size and uniform internal structure

Active Publication Date: 2021-07-09
KONFOONG MATERIALS INTERNATIONAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the preparation method has the advantages of simple process, convenient operation, and wide range of alloy components, it is suitable for large-scale industrial production, but the nickel-chromium alloy sputtering target obtained by spraying nickel-chromium powder has a high gas content, which cannot meet high-precision sputtering targets at all. Quality requirements of end industries
[0009] However, compared with conventional low chromium content (Cr content≤20wt%) nickel-chromium alloys, high chromium content (Cr content is 30-80wt%) nickel-chromium alloys have lower plastic deformation ability due to the increased C

Method used

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  • Nickel-chromium alloy sputtering target materials and hot isostatic pressing preparation method thereof

Examples

Experimental program
Comparison scheme
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Example Embodiment

[0056] Example 1

[0057] This embodiment provides a thermostatic pressure preparation method of a nickel-chromium alloy sputtering target, the heat and other static pressure preparation method comprising the steps of:

[0058] (1) Prepare the Cr content of 50% by weight of the nickel-chromium alloy powder, load the stainless steel mold, and stronger and sealing in turn;

[0059] Among them, the nickel-chromium alloy powder is mixed with chromium-chromium-chromium-chromium-chromium-chromium-chromium-chromium-chromium-based nickel-chromium-based nickel-chromium alloy powder, and the average particle size of the chromium powder is <100 μm; The mixing is carried out in a mixed powder machine, and the ball zirconium ball mass ratio is 3:10, and 30 h is mixed under argon under argon.

[0060] (2) Put the mold after the step (1), in the heating furnace, heated to 400 ° C, and control the vacuum degree or less, 6h degassing treatment;

[0061] (3) Put the mold after degasses of step (2) ...

Example Embodiment

[0063] Example 2

[0064] This embodiment provides a thermostatic preparation method of a nickel-chromium alloy sputtering target, in addition to the temperature of the heat such as the heat such as step (3) at 950 ° C for 800 ° C, other conditions and Example 1 Otamed.

Example Embodiment

[0065] Example 3

[0066] This embodiment provides a thermostatic pressure preparation method of a nickel-chromium alloy sputtering target, in addition to the temperature of 1,400 ° C, other conditions and Example 1 in addition to the temperature of the heat such as the heat such as step (3). Otamed.

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Abstract

The invention relates to a nickel-chromium alloy sputtering target materials and a hot isostatic pressing preparation method thereof. The hot isostatic pressing preparation method comprises the following steps: firstly, preparing nickel-chromium alloy powder of which Cr content is 30 percent by weight to 80 percent by weight, and filling a mould with the nickel-chromium alloy powder and sealing a mouth of the mould; then sequentially performing degassing treatment, hot isostatic pressing treatment and machining to obtain the nickel-chromium alloy sputtering target materials. According to the hot isostatic pressing preparation method disclosed by the invention, by adopting a hot isostatic pressing technology, the nickel-chromium alloy sputtering target materials with compactness being more than or equal to 99 percent, fine and small crystal grain sizes, uniform internal structure and high chromium content, can be prepared, and the phenomenon that the magnetic flux of the nickel-chromium alloy sputtering target materials is more than or equal to 99 percent also can be ensured, and therefore, the nickel-chromium alloy sputtering target materials meet the sputtering requirement in high-precision end industries such as semiconductors.

Description

technical field [0001] The invention relates to the technical field of metal materials, in particular to a nickel-chromium alloy sputtering target material and a preparation method thereof by hot isostatic pressing. Background technique [0002] Magnetron sputtering is one of the main technologies for preparing thin film materials. The ions generated by the ion source are accelerated and gathered in a vacuum to form a high-speed energy ion beam, which bombards the solid surface, and the kinetic energy exchange occurs between the ions and the solid surface atoms. , so that the atoms on the solid surface leave the solid and deposit on the surface of the substrate to form a thin film with a thickness of nanometer or micrometer. Among them, the bombarded solid is the raw material for preparing magnetron sputtering deposited films, generally called sputtering targets, which are concentrated in information storage, integrated circuits, displays, automotive rearview mirrors and oth...

Claims

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Application Information

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IPC IPC(8): C23C14/34C23C14/35B22F3/15C22C19/05C22C27/06
CPCC23C14/3414C23C14/35B22F3/15C22C19/058C22C27/06
Inventor 姚力军边逸军潘杰王学泽黄东长
Owner KONFOONG MATERIALS INTERNATIONAL CO LTD
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