Preparation method of superfine dolomite and application of superfine dolomite
A dolomite and fine powder technology, applied in chemical instruments and methods, inorganic chemistry, calcium/strontium/barium compounds, etc., can solve the problems of easy agglomeration of ultrafine powder, small application range, and difficulty in uniform dispersion
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Embodiment 1
[0039] Present embodiment is a kind of grinding aid, and the preparation process of described grinding aid comprises the following steps:
[0040] S1: Add phenol to a three-necked flask equipped with a condenser and a stirrer, then add octanoic acid and triethanolamine, and place the three-necked flask in a constant temperature oil bath at a temperature of 130°C and a stirring speed of 100r / min Stirring and reacting for 7 hours until the water is completely discharged, the crude product of intermediate 1 is obtained; the molar ratio of octanoic acid and triethanolamine is 1.6:1.0, and the dosage ratio of octanoic acid and phenol is 1g:5mL;
[0041]S2: Dissolve the crude product of intermediate 1 in isooctane to obtain the crude product solution of intermediate 1, wash the crude product solution of intermediate 1 with aqueous sodium hydroxide solution and distilled water three times respectively, and remove unreacted octanoic acid, triethanolamine and phenol , and then the crud...
Embodiment 2
[0045] Present embodiment is a kind of grinding aid, and the preparation process of described grinding aid comprises the following steps:
[0046] S1: Add phenol to a three-necked flask equipped with a condenser and a stirrer, then add octanoic acid and triethanolamine, and place the three-necked flask in a constant temperature oil bath at a temperature of 135°C and a stirring speed of 150r / min Stirring and reacting for 8 hours, until the water is completely discharged, the crude product of intermediate 1 is obtained; the molar ratio of octanoic acid and triethanolamine is 1.6:1.0, and the dosage ratio of octanoic acid and phenol is 1g:8mL;
[0047] S2: Dissolve the crude product of intermediate 1 in isooctane to obtain the crude product solution of intermediate 1, wash the crude product solution of intermediate 1 with sodium hydroxide aqueous solution and distilled water 4 times respectively, and remove unreacted octanoic acid, triethanolamine and phenol , and then the crude ...
Embodiment 3
[0051] Present embodiment is a kind of grinding aid, and the preparation process of described grinding aid comprises the following steps:
[0052] S1: Add phenol to a three-necked flask equipped with a condenser and a stirrer, then add octanoic acid and triethanolamine, and place the three-necked flask in a constant temperature oil bath at a temperature of 140°C and a stirring speed of 200r / min Stirring and reacting for 9 hours until the water is completely discharged, the crude product of intermediate 1 is obtained; the molar ratio of octanoic acid and triethanolamine is 1.6:1.0, and the dosage ratio of octanoic acid and phenol is 1g:10mL;
[0053] S2: Dissolve the crude intermediate 1 in isooctane to obtain the crude intermediate 1 solution, wash the crude intermediate 1 solution with sodium hydroxide aqueous solution and distilled water 5 times respectively, and remove unreacted octanoic acid, triethanolamine and phenol , and then the crude product solution of Intermediate ...
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