Nanoparticle composite magnetic core film and preparation method thereof

A nanoparticle and composite film technology, applied in magnetic thin films, nanostructure applications, transformer/inductor cores, etc., can solve the problems of reducing saturation magnetization and magnetic permeability, achieve low coercivity and improve resistivity , the effect of excellent soft magnetic properties

Active Publication Date: 2021-07-30
UNIV OF ELECTRONICS SCI & TECH OF CHINA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, in this type of film, although increasing the XO volume content can increase the film resistivity and reduce the coercive force, it will reduce the saturation magnetization and permeability; conversely, reducing the XO volume content can increase the saturation magnetization and permeability. rate, but at the expense of resistivity and coercivity
The above contradictions have long limited the development of high-frequency nanoparticle films.

Method used

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  • Nanoparticle composite magnetic core film and preparation method thereof
  • Nanoparticle composite magnetic core film and preparation method thereof
  • Nanoparticle composite magnetic core film and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0024] A method for preparing a nanoparticle composite magnetic core film, specifically comprising the following steps:

[0025] Step 1, adopt radio frequency magnetron sputtering method, with Fe 65 co 35 Alloys, Ti and Al 2 o 3 The patch is a composite target (through the Fe 65 co 35 3 pieces of Ti and 2 pieces of Al are pasted on the target 2 o 3 chip implementation), the target diameter is 3 inches, and FeCoTi / Al is prepared on Si(100) substrate 2 o 3 Composite thin film, sputtering power is 6W / cm 2 , the sputtering pressure is 0.17Pa, a 200Oe magnetic field is applied to induce in-plane uniaxial anisotropy, the direction of the magnetic field is parallel to the film plane, and the deposition time is controlled so that the thickness of the composite film is 200nm.

[0026] Step 2. Before annealing, Ti is not oxidized, the insulating phase content is relatively low, and the growth inhibition effect on FeCo particles is relatively weak, and the FeCo particles are rel...

Embodiment 2

[0033] A method for preparing a nanoparticle composite magnetic core film, specifically comprising the following steps:

[0034] Step 1, adopt radio frequency magnetron sputtering method, with Fe 65 co 35 Alloys, Ti and Al 2 o 3 The patch is a composite target (through the Fe 65 co 35 3 pieces of Ti and 2 pieces of Al are pasted on the target 2 o 3 chip implementation), the target diameter is 3 inches, and FeCoTi / Al is prepared on Si(100) substrate 2 o 3 Composite thin film, sputtering power is 6W / cm 2 , the sputtering pressure is 0.17Pa, a 200Oe magnetic field is applied to induce in-plane uniaxial anisotropy, the direction of the magnetic field is parallel to the film plane, and the deposition time is controlled so that the thickness of the composite film is 200nm.

[0035] Step 2, the FeCoTi / Al that step 1 obtains 2 o 3 Put the composite film into the annealing furnace, then pass in air at 1 atmosphere, raise the temperature from room temperature to 320 °C at a r...

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Abstract

A nanoparticle composite magnetic core film comprises ferromagnetic metal and X'O composite particles and an XO amorphous particle layer wrapping the surfaces of the composite particles, and the composite particles and the amorphous particle layer form a core-shell structure. The absolute value of the oxide formation enthalpy of the ferromagnetic metal is less than the absolute value of the oxide formation enthalpy of X' which is less than the absolute value of the oxide formation enthalpy of X. In the composite magnetic core film, the volume percent of ferromagnetic metal is 60%-80%, the volume percent of X'O is 10%-30%, and the volume percent of XO is 10%-30%. According to the nanoparticle composite magnetic core film provided by the invention, firstly, a structure in which the surface of an MX' alloy is coated with an XO oxide layer is formed through magnetron sputtering, and the purpose of increasing the resistivity of the film is achieved with relatively low volume content; and secondly, annealing treatment is carried out in an oxidizing atmosphere, so that X' is oxidized, magnetic particles are separated out and refined, random anisotropy is introduced, and the coercive force of the film is effectively reduced.

Description

technical field [0001] The invention relates to a high-frequency nanocomposite magnetic core film suitable for magnetic devices such as thin film inductors and transformers and a preparation method thereof. Background technique [0002] The development of electronic information technology requires electronic devices to be more miniaturized and integrated. At the same time, in the process of miniaturization and thin filming of the components themselves, as the most important thin film inductors in micromagnetic devices, they can especially integrate with semiconductor devices. The thin film inductors integrated together have broad application prospects in the modern information field. With the development of electronic communication technology, especially the arrival of the 5G era, integrated magnetic devices based on thin film core materials are developing towards high frequency, which puts forward higher requirements for the high frequency performance of soft magnetic thin ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F10/12H01F10/18H01F10/187H01F41/18H01F41/22H01F41/30H01F27/24
CPCH01F10/12H01F10/18H01F10/187H01F41/183H01F41/22H01F41/30H01F27/24
Inventor 白飞明邹想张怀武
Owner UNIV OF ELECTRONICS SCI & TECH OF CHINA
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