A kind of high-strength plate with metal coating and preparation method thereof
A metal coating, high-strength technology, applied in metal material coating process, sputtering coating, vacuum evaporation coating and other directions, can solve the problems of difficult processing, high maintenance cost, easy to attach fingerprints, etc., to improve mechanical properties and heat resistance, good anti-fingerprint performance, and the effect of improving smoothness
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Embodiment 1
[0047] (1) Preparation of substrate:
[0048] Get the following weight components for subsequent use: 74 parts of glycidol, 216 parts of acrylic acid, 0.37 parts of p-phenol, 0.74 parts of dimethylbenzylamine, 7 parts of zinc chloride;
[0049] Take glycidol, add 10% mass of acrylic acid in a nitrogen atmosphere and mix evenly, add p-phenol and dimethylbenzylamine, heat up to 70°C, slowly add 35% mass of acrylic acid, and react until the viscosity of the system is no longer. When changing again, add acrylic acid, zinc chloride and toluene of 10% by mass components, heat the temperature to 115 °C, keep the temperature for the reaction, add acrylic acid and toluene of the remaining components, and after the reaction is completed, vacuum dry and cool to prepare unsaturated polymer. Ester, adding initiator, pouring into mold, hot pressing, hot pressing process: pressure 7kgf / cm 2 , the pressing temperature is 80°C, the pressing time is 100min, the vacuum is 700mmHg, take out and ...
Embodiment 2
[0062] (1) Preparation of substrate:
[0063] Get the following weight components for subsequent use: 92 parts of glycidol, 270 parts of acrylic acid, 0.46 parts of p-phenol, 0.92 parts of dimethylbenzylamine, 9 parts of zinc chloride;
[0064] Take glycidol, in a nitrogen atmosphere, add 15% mass of acrylic acid and mix evenly, add p-phenol and dimethylbenzylamine, heat up to 75°C, slowly add 37% mass of acrylic acid, and react until the viscosity of the system is no longer. When changing again, add acrylic acid, zinc chloride and toluene with 13% mass components, heat up to 117°C, keep the temperature for reaction, add acrylic acid and toluene of the remaining components, after the reaction is completed, vacuum dry and cool to prepare unsaturated polymer. Ester, add initiator, pour into mold, hot press, hot pressing process is: pressure 13kgf / cm 2 , the pressing temperature is 100°C, the pressing time is 125min, the vacuum is 730mmHg, take out and cool to obtain the substra...
Embodiment 3
[0077] (1) Preparation of substrate:
[0078] Get the following weight components for subsequent use: 111 parts of glycidol, 324 parts of acrylic acid, 0.55 parts of p-phenol, 1.11 parts of dimethylbenzylamine, 11 parts of zinc chloride;
[0079] Take glycidol, in a nitrogen atmosphere, add 20% mass of acrylic acid and mix evenly, add p-phenol and dimethylbenzylamine, heat up to 80°C, slowly add 40 mass% of acrylic acid, and react until the viscosity of the system is no longer. When changing again, add acrylic acid, zinc chloride and toluene of 15% mass components, heat up to 120 ° C, keep the temperature for the reaction, add acrylic acid and toluene of the remaining components, after the reaction is completed, vacuum dry and cool to prepare unsaturated polymer. Ester, adding initiator, pouring into mold, hot pressing, hot pressing process: pressure 7~20kgf / cm 2 , the pressing temperature is 120°C, the pressing time is 150min, the vacuum is 760mmHg, take out and cool to obta...
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