Nano preservative wood protective agent and preparation method thereof
A protective agent and preservative technology, applied in wood treatment, impregnated wood, wood impregnation, etc., can solve the problems of poor fungal decay inhibition effect, inability to effectively avoid insect damage, and low safety in use, so as to improve dispersion uniformity and stability Anti-corrosion and anti-oxidation ability, high safety effect
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Embodiment 1
[0030] A kind of nano preservative wood protective agent
[0031] Prepared by:
[0032] S10, 1.0kg of boric acid is used to make an aqueous solution with a mass fraction of 15%, keep it warm at 35°C, add 0.5kg of dodecyldimethylbenzyl ammonium chloride, stir at a speed of 150r / min for 5min, and let it stand for 1h to obtain mixture;
[0033] S20, S10 mixed solution is stirred at the speed of 300r / min while adding 1.2kg nano-zinc oxide, 0.8kg nano-tin dioxide and 1.2kg sodium hydroxymethyl cellulose, and continues to stir for 15min to obtain component A solution;
[0034] In the above operation, the nano-zinc oxide, nano-tin dioxide and sodium hydroxymethyl cellulose were uniformly mixed in advance and ground for 60 minutes.
[0035] S30, 8.4kg of isobutylene triethoxysilane and 3.8kg of n-butanol, 4.0kg of polyethylene glycol, and 2.8kg of polyvinyl alcohol were mixed ultrasonically for 30 minutes at a temperature of 30°C, and then 0.6kg of sorbitol was added. Shake and mix...
Embodiment 2
[0039] A kind of nano preservative wood protective agent
[0040] Prepared by:
[0041] S10, 1.5kg of boric acid is used to make an aqueous solution with a mass fraction of 35%, keep it warm at 38°C, add 3.5kg of dodecyldimethylbenzyl ammonium chloride, stir at a speed of 350r / min for 10min, and let it stand for 2h to obtain mixture;
[0042]S20, S10 mixed solution is stirred with the speed of 500r / min while adding 3.4kg nano-zinc oxide, 2.2kg nano-tin dioxide and 1.6kg sodium hydroxymethyl cellulose, continue to stir for 20min, obtain component A solution;
[0043] In the above operation, the nano-zinc oxide, nano-tin dioxide and sodium hydroxymethyl cellulose were uniformly mixed in advance and ground for 90 minutes.
[0044] S30, 10.6kg of isobutylene triethoxysilane and 6.4kg of n-butanol, 6.0kg of polyethylene glycol, and 5.6kg of polyvinyl alcohol were mixed ultrasonically for 45 minutes at a temperature of 40°C, and then 0.8kg of sorbitol was added. Shake and mix for...
Embodiment 3
[0048] A kind of nano preservative wood protective agent
[0049] Prepared by:
[0050] S10, 1.2kg of boric acid was prepared into an aqueous solution with a mass fraction of 18%, and the temperature was kept at 36°C, 1.4kg of dodecyldimethylbenzyl ammonium chloride was added, stirred at a speed of 180r / min for 6min, and allowed to stand for 1.2h. to obtain a mixed solution;
[0051] S20, S10 mixed solution is stirred at the speed of 350r / min while adding 1.4kg nanometer zinc oxide, 1.0kg nanometer tin dioxide and 1.3kg sodium hydroxymethyl cellulose, continue stirring for 16min, obtain component A solution;
[0052] In the above operation, nanometer zinc oxide, nanometer tin dioxide and sodium hydroxymethylcellulose were mixed uniformly in advance and ground for 70 minutes.
[0053] S30, 8.8kg of isobutylene triethoxysilane and 4.0kg of n-butanol, 4.5kg of polyethylene glycol, and 3.4kg of polyvinyl alcohol were mixed ultrasonically for 35 minutes at a temperature of 32°C, ...
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