Preparation method for producing water-soluble dietary fibers rich in gamma-aminobutyric acid by using soy sauce residues as raw materials
A technology of dietary fiber and aminobutyric acid, which is applied in the field of food processing, can solve the problems of complex GABA purification technology, safety problems of Escherichia coli, and low GABA content, and achieve good market application value, low cost, and low reagent consumption.
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Embodiment 1
[0032] A preparation method for producing water-soluble dietary fiber rich in gamma-aminobutyric acid by using soy sauce residue as raw material, specifically comprising the following steps:
[0033] 1. Put 10kg of dried soy sauce residue into the extraction kettle, use butane as the extraction agent, under the conditions of extraction temperature of 50°C and extraction pressure of 0.8MPa, flow through the extraction kettle at a flow rate of 100L / h- countercurrently, Continuous extraction for 60 minutes; after the extracted butane enters the desorption kettle, the desorption temperature is 75°C, the desorption pressure is 0.2MPa, and the defatted soy sauce residue is collected.
[0034] 2. Add the defatted soy sauce residue obtained above into MES-TRIS buffer solution, the ratio of material to liquid is 1:10, mix well, and then grind in a colloid mill for 20 minutes; add 10 g of papain, and perform enzymatic hydrolysis for 2 hours, and the temperature of the enzymatic hydrolysi...
Embodiment 2
[0038] A preparation method for producing water-soluble dietary fiber rich in gamma-aminobutyric acid by using soy sauce residue as raw material, specifically comprising the following steps:
[0039]1. Put 10kg of dried soy sauce residue into the extraction kettle, use butane as the extraction agent, under the conditions of extraction temperature of 60°C and extraction pressure of 0.8MPa, flow through the extraction kettle countercurrently at a flow rate of 100L / h-, Continuous extraction for 60 minutes; after the extracted butane enters the desorption kettle, the desorption temperature is 75°C, the desorption pressure is 0.2MPa, and the defatted soy sauce residue is collected.
[0040] 2. Add the defatted soy sauce residue obtained above into MES-TRIS buffer solution, the ratio of material to liquid is 1:10, mix well, and then grind in a colloid mill for 40 minutes; add 10 g of papain, enzymatic hydrolysis for 3 hours, and the temperature of the enzymatic hydrolysis water bath ...
Embodiment 3
[0044] A preparation method for producing water-soluble dietary fiber rich in gamma-aminobutyric acid by using soy sauce residue as raw material, specifically comprising the following steps:
[0045] 1. Put 10kg of dried soy sauce residue into the extraction kettle, use butane as the extraction agent, under the conditions of extraction temperature of 50°C and extraction pressure of 0.8MPa, flow through the extraction kettle at a flow rate of 100L / h- countercurrently, Continuous extraction for 60 minutes; after the extracted butane enters the desorption kettle, the desorption temperature is 75°C, the desorption pressure is 0.2MPa, and the defatted soy sauce residue is collected.
[0046] 2. Add the defatted soy sauce residue obtained above into MES-TRIS buffer solution, the ratio of material to liquid is 1:10, mix well, and then grind in a colloid mill for 60 minutes; add 15g of papain, and enzymatically hydrolyze for 2 hours, and the temperature of the enzymatic hydrolysis wate...
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