Alkali-free substrate glass and thinning method thereof

A glass thinning and alkali-free technology, which is applied in the direction of manufacturing tools, grinding devices, grinding machine tools, etc., can solve the problems of uneven glass surface etching, glass surface roughness, and affecting product performance, so as to achieve the effect of improvement and realize the glass Thickness, wettability improvement effect

Pending Publication Date: 2022-01-04
IRICO DISPLAY DEVICES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, it is usually necessary to thin the relatively thick substrate glass. The commonly used thinning methods are divided into chemical etching thinning and mechanical polishing thinning. The existing substrate glass is very hard to use due to its high surface hardness. Therefore, chemical etching is often used to thin the glass, that is, the chemical etching solution is sprayed through the spray device to thin the glass, but this method will cause uneven etching on the glass surface and cause the glass surface to be rough, affecting product performance.

Method used

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  • Alkali-free substrate glass and thinning method thereof
  • Alkali-free substrate glass and thinning method thereof
  • Alkali-free substrate glass and thinning method thereof

Examples

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Effect test

Embodiment 1

[0035] A kind of alkali-free substrate glass, by mass percentage, comprises the following components: 60.4% SiO 2 , 17.1% Al 2 o 3 , 12.8% B 2 o 3 , 1.4% MgO, 6.7% CaO, 1.2% SrO, 0% BaO, and 0.1% SnO 2 .

[0036] The alkali-free substrate glass with a thickness of 0.7mm is prepared by the preparation method of the alkali-free substrate glass of the present invention.

[0037] A method for thinning the non-alkali substrate glass, the non-alkali substrate glass in the present embodiment is thinned by the following steps,

[0038] S1: Thinning by chemical etching: immerse the alkali-free substrate glass in this embodiment into a chemical etching solution containing 25% hydrofluoric acid, 10% glacial acetic acid, and 3% sodium dodecylsulfonate Corrode in medium for 30min, take out the non-alkali substrate glass, use alcohol and pure water for ultrasonic cleaning and drying, use a spiral micrometer to measure the thickness until the thickness of the glass sheet reaches 0.5mm....

Embodiment 2

[0042] A kind of alkali-free substrate glass, by mass percentage, comprises the following components: 61.2% SiO 2 , 18.4% Al 2 o 3 , 10.3% B 2 o 3 , 1.4% MgO, 7.5% CaO, 1.0% SrO, 0% BaO, and 0.2% SnO 2 .

[0043] The alkali-free substrate glass with a thickness of 0.7mm is prepared by the preparation method of the alkali-free substrate glass of the present invention.

[0044] A method for thinning the non-alkali substrate glass, the non-alkali substrate glass in the present embodiment is thinned by the following steps,

[0045] S1: Thinning by chemical etching: immerse the alkali-free substrate glass in this embodiment in a chemical etching solution containing 27% hydrofluoric acid, 11.5% glacial acetic acid, and 3.2% sodium dodecyl sulfate After eroding for 28.5 minutes, take out the alkali-free substrate glass, clean and dry it ultrasonically with alcohol and pure water, repeat step S1 once, and measure the thickness with a spiral micrometer until the thickness of the ...

Embodiment 3

[0049] A kind of alkali-free substrate glass, by mass percentage, comprises the following components: 60.8% SiO 2 , 18.3% Al 2 o 3 , 4.3% B 2 o 3 , 1.9% MgO, 4.1% CaO, 2.1% SrO, 8.3% BaO, and 0.2% SnO 2 .

[0050] The alkali-free substrate glass with a thickness of 0.7mm is prepared by the preparation method of the alkali-free substrate glass of the present invention.

[0051] A method for thinning the non-alkali substrate glass, the non-alkali substrate glass in the present embodiment is thinned by the following steps,

[0052] S1: Thinning by chemical etching: the alkali-free substrate glass in this embodiment is immersed in a chemical etching solution containing 26.8% hydrofluoric acid, 12% glacial acetic acid, and 3.8% sodium dodecylbenzenesulfonate. Corrode in the solution for 27 minutes, take out the alkali-free substrate glass, use alcohol and pure water for ultrasonic cleaning and drying, and use a spiral micrometer to measure the thickness until the thickness of...

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Abstract

Alkali-free substrate glass comprises the components in percentage by mass: 58.9% to 62.5% of SiO2, 14.2% to 18.4% of Al2O3, 4.3% to 13.7% of B2O3, 1.4% to 1.9% of MgO, 4.1% to 7.6% of CaO, 1.0% to 2.1% of SrO, 0 to 8.3% of BaO and 0.1% to 0.2% of SnO2. The thinning method comprises the following steps: immersing the alkali-free substrate glass into a chemical etching solution composed of hydrofluoric acid, a glacial acetic acid surfactant and the balance being water, thinning the alkali-free substrate glass to 0.4 mm-0. 5mm, taking out the alkali-free substrate glass, and carrying out ultrasonic cleaning and drying; and placing the alkali-free substrate glass on a grinding disc of a grinding and polishing machine, and carrying out mechanical polishing, thinning the alkali-free substrate glass to 0.3 mm-0.35 mm, and thus obtaining the flexible substrate glass. The alkali-free substrate glass is reasonable in composition, the specific modulus value of the prepared alkali-free glass is moderate, the glass has good flexibility, the thinning method is convenient to operate, the alkali-free substrate glass with the thickness of 0.7 mm is thinned by combining two modes of chemical etching thinning and mechanical polishing thinning, and the flexible substrate glass with smooth surface and bendable performance is obtained.

Description

technical field [0001] The invention belongs to the field of flexible substrate glass manufacturing, and relates to an alkali-free substrate glass and a preparation method thereof. Background technique [0002] With the improvement of living standards, people's requirements for electronic display devices are developing in the direction of thinner, smarter, and more flexible, especially in recent years, electronic wearable devices, bendable smart phones and more realistic Curved surface display technology has given new flexible performance requirements to the ultra-thin glass that is the basis of electronic displays. According to flexible display products, the display screen can be divided into four types, namely flexible display with paper quality, flexible display with micro-curvature, foldable display and roll-up flexible display. The latter two types of flexible displays have very high requirements on the flexibility of the glass used, while the first two types of flexib...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C3/091C03C15/02B24B37/34B24B37/30B24B37/10
CPCC03C3/091C03C15/02B24B37/10B24B37/30B24B37/34
Inventor 王答成兰静曾召孔令歆郭静
Owner IRICO DISPLAY DEVICES
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