Blue color weakness correction lens and preparation method thereof
A kind of color blindness and lens technology, which is applied in the field of color vision correction optical materials and preparations, can solve problems such as vision loss, inability to distinguish, difficult to accept the appearance of bright red and green, and achieve the effect of improving vividness, sensitive spectral response, and good rigidity
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Embodiment 1
[0060] Embodiment 1: Preparation of organic / inorganic nanocomposite microspheres and color vision correction lenses
[0061] (1) Preparation of organic / inorganic nanocomposite microspheres:
[0062] 1. Take 2.5g of emulsifier RF-345 and add it to 1100g of pure water. After it is completely dissolved, add 30g of nano-copper oxide, add 120g of sodium acetate saturated aqueous solution dropwise within 70min, and then add 20g of cross-linking agent DAP; Enter nitrogen, add 145g of dichloromethane solvent containing spiropyran compound (formula I) (spiropyran 35g solvent 110g), add methyl acrylate monomer 18g and ethyl acrylate monomer 10g, stir and heat up to 65 ° C, add Initiator ammonium persulfate 0.1g, keep warm for 16h, filter, wash and dry to obtain acrylate / spiropyran / copper oxide nanospheres. The yield was 82%.
[0063] 2. The product prepared in step 1 is observed with a transmission electron microscope, as figure 2 As shown, it can be seen that the appearance is sphe...
Embodiment 2
[0069] Embodiment 2: Preparation of color vision correction lens
[0070] (1) Preparation of organic / inorganic nanocomposite microspheres:
[0071]i. Take 2g of emulsifier sodium dodecylbenzene sulfonate and add it to 1000g of pure water. After it is completely dissolved, add 26g of nano-titanium oxide, add 140g of sodium acetate saturated aqueous solution dropwise within 70min, and then add 20g of crosslinking agent butyl acrylate ; Feed nitrogen into the reactor, add 130 g of dichloromethane solvent containing spiropyran compound (formula I) (100 g of spiropyran 30 g solvent), add 26 g of ethyl acrylate monomer, stir and heat up to 70 ° C, add trigger Add 0.1 g of sodium persulfate, keep warm for 16 hours, filter, wash, and dry to obtain acrylate / spiropyran / titanium oxide nanospheres. The yield was 78%.
[0072] ii. the product prepared in step (i) is observed through a transmission electron microscope, such as image 3 As shown, it can be seen that the appearance is sphe...
Embodiment 3
[0077] Embodiment 3: the nanocomposite microsphere structure analysis that embodiment 1 and embodiment 2 prepare
[0078] Carry out N to the nanocomposite microsphere sample that embodiment 1-2 prepares 2 Adsorption-desorption isotherm detection was carried out to analyze the structural characteristics of the nano-microspheres, and the results are shown in Figure 6. Wherein P1, P2 represent the nanocomposite microsphere sample that embodiment 1, embodiment 2 prepare respectively, Figure 6a for N 2 Adsorption-desorption isotherm, the isotherm type of the sample with 10h hydrothermal reaction time is type IV, at P / P 0 There is a hysteresis loop at 0.4-1.0, indicating the existence of mesopores. Figure 6b It is a pore size distribution curve. There is an obvious raised peak at 3nm, and there is no raised peak after 5nm, indicating that the pore size is small, and the pore size is about 3nm. The mesopores in the sample are formed by the aggregation of nanoparticles. All thes...
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