Application of combination of multiple serum tumor markers in specific early diagnosis and curative effect monitoring and detection of pancreatic cancer
A tumor marker and early diagnosis technology, applied in the field of medical detection, can solve the problems of poor specificity, increase, and increase of CA19-9, and achieve the effect of large clinical benefits
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Embodiment 1
[0040] Embodiment 1: preparation kit of the present invention
[0041] The main components and preparation of the kit of the present invention:
[0042] R1 reagent:
[0043] Fluorescein isothiocyanate (FITC)-labeled anti-MMP-II antibody, antibody concentration range 0.5-2.5μg / mL, bovine serum albumin and preservative Tris buffer (concentration 0.1mol / L, pH=8.0).
[0044] Fluorescein isothiocyanate (FITC)-labeled anti-MIC-1 antibody, antibody concentration range 0.2-1.2μg / mL, bovine serum albumin and preservative Tris buffer (concentration 0.1mol / L, pH=8.0).
[0045] Fluorescein isothiocyanate (FITC)-labeled anti-REG4 antibody, antibody concentration range 0.2-1.2μg / mL, bovine serum albumin and preservative Tris buffer (concentration 0.1mol / L, pH=8.0).
[0046]Fluorescein isothiocyanate (FITC)-labeled anti-LAMC2 antibody, antibody concentration range 0.5-1.5μg / mL, bovine serum albumin and preservative Tris buffer (concentration 0.1mol / L, pH=8.0)1) Fluorescein thiocyanate (FI...
Embodiment 2
[0103] Embodiment 2: the detection method of embodiment 1 kit
[0104] The patent kit adopts magnetic particle chemiluminescence immunoassay method, and is suitable for automatic magnetic particle chemiluminescence analyzer. The detection principle is to mix and incubate the sample to be tested, reagent 1 (R1), and reagent 2 (R2), and a pair of antibodies labeled with fluorescein isothiocyanate (FITC) in R1 and alkaline phosphatase (ALP) in R2 The biomarker monoclonal antibody specifically binds to the biomarker antigen molecule in the sample to form an immune complex. The immune complex and the magnetic separation reagent (M) are mixed and incubated, and the immune complex is further captured by the anti-FITC antibody coupled on the surface of the magnetic particle and adsorbed to the surface of the magnetic particle. After washing and removing unbound antibodies and impurities, a luminescent substrate is added, ALP catalyzes the substrate to emit light, and the relative lum...
Embodiment 3
[0113] Example 3: When the kit of the present invention detects serum samples from healthy people, patients with chronic pancreatitis-related diseases, pancreatic cancer, and other malignant tumors of the digestive tract, the sensitivity, specificity and ROC curve analysis of the performance indicators of the kit sample.
[0114] The clinical samples included in this patent come from the remaining serum samples after clinical tests of inpatients or outpatients in the Cancer Hospital of the Chinese Academy of Medical Sciences, Henan Provincial People's Hospital, Qingdao Municipal Hospital and other hospitals. The sample volume is 200ul ~ 500ul, and the sample- 80 ℃ w storage time 2 to 3 years. The case information of each sample is complete, clear and traceable. The distribution information of the sample population is as follows:
[0115]
[0116] Optimal combination of multi-index combined detection in early diagnosis of pancreatic cancer:
[0117] Surgical resection is ...
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