Plasma-treated chitosan antibacterial fiber and preparation method thereof
A plasma and antibacterial fiber technology, applied in the field of textile fabrics, can solve the problems of damaging fiber evenness and mechanical properties, increasing impurities, and being easily oxidized, achieving low cost, short process, and strong antibacterial effect
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[0029] The invention provides a preparation method of plasma-treated chitosan antibacterial fiber, comprising the following steps: S1) performing plasma treatment on the fiber to obtain the treated fiber; S2) spraying the chitosan antibacterial solution by atomizing Cover the treated fiber, and obtain plasma treated chitosan antibacterial fiber after high temperature treatment; the chitosan antibacterial solution includes chitosan, amino silicone oil and water.
[0030] Wherein, the present invention has no special limitation on the sources of all raw materials, which can be commercially available or self-made.
[0031] The fiber is subjected to plasma treatment to obtain the treated fiber; the fiber is preferably a single-strand fiber; its type is preferably nylon, polyester or acrylic fiber, more preferably polyester; the plasma treatment is preferably low-temperature plasma treatment; The power of the plasma treatment is preferably 50-100W; the plasma treatment is preferabl...
Embodiment 1
[0045] The preparation method of 75D / 72F plasma treatment chitosan polyester antibacterial fiber mainly includes the following steps:
[0046] 1.1 Chitosan powder material preparation: mainly use crab shells and shrimp shells as raw materials to finally obtain chitosan with a particle size of 80 nanometers and a molecular weight of 10,000 through processes such as shell removal, protein removal, inorganic salt removal, and deacetylation. Sugar antibacterial liquid material.
[0047] 1.2 Plasma treatment: First, low-temperature plasma treatment is applied to the polyester single-strand fiber, so that free radicals such as -OH, -COOH, and -C=O are generated on the surface of the polyester fiber).
[0048] 1.3 Antibacterial treatment: Prepare the chitosan prepared in 1.1 as an antibacterial liquid material and apply it to a single yarn by atomization spraying, and then react with free radicals generated on the surface of polyester fibers through high temperature reaction and dryi...
Embodiment 2
[0064] The preparation method of 50D / 48F plasma treatment chitosan polyester antibacterial fiber mainly includes the following steps:
[0065] 2.1 Chitosan powder material preparation: mainly use crab shells and shrimp shells as raw materials to finally obtain chitosan with a particle size of 80 nanometers and a molecular weight of 11,000 through processes such as shell removal, protein removal, inorganic salt removal, and acetylation. Sugar antibacterial liquid material.
[0066] 2.2 Plasma treatment: first, low-temperature plasma treatment is applied to the polyester single-strand fiber, so that free radicals such as -OH, -COOH, and -C=O are generated on the surface of the polyester fiber).
[0067] 2.3 Antibacterial treatment: Prepare the chitosan prepared in 2.1 as an antibacterial liquid material and apply it to a single yarn by atomization spraying, and then react with free radicals generated on the surface of polyester fibers through high temperature reaction and drying...
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