Polypyrrole wood foam for solar landfill leachate treatment and preparation method of polypyrrole wood foam
A technology of landfill leachate and polypyrrole, which is applied in the direction of contaminated groundwater/leachate treatment, water/sewage treatment, chemical instruments and methods, etc., can solve the problems of high cost, high cost and easy pollution of the environment of solar drives, etc. Achieve the effect of reducing production cost and production difficulty, and good processing effect
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Embodiment example 1
[0036] The preparation method of polypyrrole wood foam is as follows:
[0037] (1) raw material grinding: the raw material used in the present invention is woody wood flour. Pour it into clean water for heating and stirring, and then perform mechanical wet grinding again, so that the diameter of the wood particles is close to the nanometer level.
[0038] (2) In situ polymerization: the K 2 S 2 o 8 Pour the solution into the woody suspension, heat and stir in a water bath for 2 hours, then lower the temperature of the water bath to about 10°C, continue to stir and cool down for 30 minutes, then slowly inject the pyrrole solution into the woody suspension under stirring, and continue stirring 2h, and then stand still for 6h, so that the pyrrole is fully polymerized on the wood in situ, and the wood turns black.
[0039] (3) Foam forming: Take 20ml of the suspension prepared in (2) and put it into a 50ml round-bottomed plastic centrifuge tube, use temperature gradient adjust...
Embodiment example 2
[0042] The difference between this implementation case and the first implementation case lies in step (2).
[0043] The quality of pyrrole in the implementation case 1 accounts for 7% of the wood quality. In this implementation case, the quality of pyrrole added accounts for 20%, 15%, 10%, 5% and 2% of the wood quality respectively, and the solid content of wood remains at 13%. The rest of the preparation scheme remains unchanged, and the experimental sequence with pyrrole mass as the variable is formed to carry out the indoor solar landfill leachate treatment experiment.
Embodiment example 3
[0045] The difference between this implementation case and the first implementation case lies in step (3).
[0046]In this implementation case, put 20ml of the prepared suspension into a 50ml round-bottomed plastic centrifuge tube, seal the mouth of the centrifuge tube with plastic wrap, turn the centrifuge tube upside down, gently tap all the suspension into the bottom, and the rest of the steps Same as Example 1, a 3D structure of a cylinder with a flat top can be prepared for indoor solar landfill leachate treatment experiments.
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