Active peptide, active peptide composition and application of active peptide composition in preparation of products with anti-aging effect
A technology of active peptides and compositions, applied in the field of biomedicine, can solve problems such as aging, and achieve the effect of convenient operation, wide application prospects, and excellent anti-aging activity
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Embodiment 1
[0034] Example 1 Preparation of active peptide
[0035] (1) Take 200 mg of Fmoc-His Wang Resin and put it in a solid-phase synthesis tube, add N,N-dimethylformamide (DMF) and let it stand for 40 minutes to fully swell the resin, filter off the solvent, and then add piperidine DMF solution, and the solvent was filtered off after shaking. Dissolve Fmoc-Ser-OH, 1-hydroxybenzotriazole, O-benzotriazole-tetramethylurea hexafluorophosphate in DMF, add N,N-diisopropylethylamine and mix well After being protected from light, it has been activated, and added to the resin, stirred with nitrogen at 25° C. for 2 hours, filtered with suction, washed with DMF and dichloromethane in turn, and drained the solvent. Repeat the above steps, add the activated Fmoc-His-OH, Fmoc-Glu-OH, Fmoc-Trp-OH, Fmoc-Leu-OH to the resin in turn, blow and stir with nitrogen at 25°C, wash the resin after the reaction is complete, The obtained filtrate was subjected to rotary evaporation to obtain a precipitate, ...
experiment example
[0043] In order to evaluate the BLO-1, BLO-2, BLO-3 and active peptide composition (the composition of BLO-1, BLO-2 and BLO-3 molar ratio 1:1:1 composition) prepared in Example 1 of the present invention , referred to as TBLO) biological activity, the following effect experiment example. The BaP in the following experimental examples is benzo[a]pyrene.
[0044] (1) Place 10 pregnant adult nematodes on NGM plates, inoculate Escherichia coli strain OP50 and lay eggs for about 5 hours to obtain synchronized populations. Then, BLO-1, BLO-2, BLO-3, TBLO enhanced nematode resistance to oxidative stress was assessed using L4 larval nematodes at 20°C. Nematodes were incubated for 1 day on treated plates containing 0.10 mM BaP, then transferred to NGM / OP50 plates containing 5 mg / mL BLO-1 or BLO-2 or BLO-3 or TBLO.
[0045] (2) Motility was assessed using 1-day-old adult C. elegans at 20°C. C. elegans were cultured on treated plates containing 0.10 mM BaP for 1 day and transferred to...
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