Compound for preventing, preventing or treating microbial infection as well as preparation method and application thereof
A compound and microbial technology, applied in the field of bacteria, preventable treatment of viruses, preventive treatment of viruses, fungal infectious diseases, and complexes of bacterial and fungal infections, can solve the problem of not being able to be widely killed and prevented, and the lack of antibacterial Toxic side effects and other issues
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[0266] The complex of the present invention is prepared by combining a carbon chain-providing compound such as a fatty acid with proteins, polypeptides, oligopeptides, oligosaccharides, monosaccharides, disaccharides, oligonucleotides, vitamins, water-soluble polymers, water-soluble Polyamino acids and / or polysaccharide molecules react, or add linkers such as PEG, N-hydroxybutenimide, amino acids, succinic acid, butadienoic acid, glutaric acid, hexamethylene diacid, Any one or two or more of carbamates, short peptides, etc. and their derivatives are reacted to obtain a reaction mixture; in a preferred scheme, the reaction mixture is further purified to separate and obtain a purified reaction product (in The "purified reaction product" is also referred to as "reaction-obtained compound" in this application, and the term "reaction-obtained compound" refers to the substance remaining after the reaction mixture is separated by purification means to remove unreacted substances, whic...
Embodiment 1
Example 1 Preparation and characterization of human serum albumin / bovine serum albumin grafted fatty acid complex (acting part + macromolecular water-soluble part / binding part)
The reaction formula example 1-1 is as follows:
In this embodiment, the molar ratio of fatty acid and albumin is 10:1, and the fatty acid is selected from fumaric acid, octanoic acid, undecanoic acid, hexadecenoic acid, oleic acid, linoleic acid, linolenic acid and eicosapentaenoic acid respectively. (EPA), docosahexaenoic acid (DHA), and triaconoic acid react with serum albumin, respectively. The molar ratio of catalyst to fatty acid is 1:1, and the catalyst is 1-ethyl-(3-dimethylaminopropyl) carbodiimide (EDC), N-hydroxysulfosuccinimide (sulfo-NHS) . The reaction process is as follows:
Accurately weigh 0.36 mmol of fatty acid, 0.36 mmol of EDC, and 0.36 mmol of sulfo-NHS; add acid to catalyze and activate the carboxyl group to form activated fatty acid; stir and activate under ice bath for 15...
Embodiment 2
[0322] Example 2 Preparation and characterization of bovine serum albumin grafted fatty acid complex (acting part + macromolecular water-soluble part / binding part)
Accurately weigh 0.36 mmol of oleic acid; 0.36 mmol of EDC; 0.36 mmol of sulfo-NHS with acid to catalyze and activate the carboxyl group to obtain activated oleic acid; stir and activate under ice bath for 10 min. Precisely weigh 0.018 mmol of bovine serum albumin (calculated as 1.2 g by mass), dissolve it in 5 ml of PBS solution, add NaOH solution to adjust the pH to neutrality, and stir evenly to obtain a serum albumin solution. The serum albumin solution was added to the activated oleic acid under stirring, and the stirring reaction was continued overnight in an ice bath to obtain the initial dissolution of oleic acid-albumin with an oleic acid concentration of 72 mM. The above solution was precipitated with ice acetone, then ethanol was used to remove fatty acids that did not participate in the reaction, and sm...
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