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Evaporative crystallization process for calcium formate production

An evaporative crystallization and calcium formate technology, which is applied in solution crystallization, separation/purification of carboxylic acid compounds, preparation of carboxylate, etc., can solve the problems of heavy metals, arsenic, and calcium carbonate impurities that are easy to remain, lack of synthetic liquid purification steps, and difficult to guarantee Product quality and other issues, to achieve the effect of improving operational safety, pure white color, and uniform particles

Pending Publication Date: 2022-07-15
阳城县正达新型材料股份有限公司
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Problems solved by technology

[0003] The methods for industrialized production of calcium formate are mainly calcium carbonate method and calcium hydroxide method, wherein, in the preparation of the above methods, there is a lack of purification steps for the synthetic liquid, and impurities such as heavy metals, arsenic, and calcium carbonate are likely to remain in the raw materials, and it is difficult to guarantee the quality of the product. quality, therefore, the present invention proposes a kind of evaporative crystallization process for the production of calcium formate to solve the problems existing in the prior art

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  • Evaporative crystallization process for calcium formate production

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Embodiment Construction

[0034] In order to deepen the understanding of the present invention, the present invention will be described in further detail below with reference to the embodiments. The embodiments are only used to explain the present invention and do not constitute a limitation on the protection scope of the present invention.

[0035] according to figure 1 As shown, the present embodiment proposes a kind of evaporative crystallization process for calcium formate production, comprising the following steps:

[0036] Step 1: Gas Treatment

[0037] The gas is drawn from the gas generator to the purification device, and the gas is treated by the purification device to increase the content of carbon monoxide and reduce the content of carbon dioxide and other impurities. The volume percentage of the product is reduced to below 2%;

[0038] Step 2: Gas Compression

[0039] Pass the purified gas into the gas compressor, and use the gas compressor to compress the gas to obtain gas liquid;

[0...

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Abstract

The invention provides an evaporative crystallization process for calcium formate production, and relates to the technical field of calcium formate production, and the evaporative crystallization process comprises the following steps: coal gas treatment, coal gas compression, calcium oxide weighing, tubular reaction, impurity removal, evaporative crystallization, centrifugal drying and cooling packaging. According to the method, the step of removing impurities is carried out after liquid synthesis and before evaporative crystallization, calcium carbonate in the synthesis liquid is firstly removed through heating, the calcium carbonate is decomposed into calcium oxide and carbon dioxide, the calcium oxide is left in the synthesis liquid to continue to participate in the reaction, the carbon dioxide escapes, and then the heavy metal capture microspheres are prepared. Impurities such as heavy metal, arsenic and calcium carbonate are captured and removed in the purification process, so that the product quality is ensured, and the produced calcium formate product is proved to have the content of 99% or above, the purity is high, and the color is pure white.

Description

technical field [0001] The invention relates to the technical field of calcium formate production, in particular to an evaporation crystallization process for calcium formate production. Background technique [0002] Calcium formate is an organic substance with the molecular formula C 2 H 2 O 4 Ca, used as a feed additive, is suitable for all kinds of animals, and has the functions of acidification, mildew resistance, antibacterial, etc. It is also used in industry as an additive for concrete, mortar, leather tanning or as a preservative. The amount of calcium formate varies with temperature. It will gradually increase as it decreases, even if it is applied at 0.3-0.5% in summer, it will have an obvious early-strength effect; [0003] The methods for industrial production of calcium formate are mainly the calcium carbonate method and the calcium hydroxide method, wherein, in the preparation of the above-mentioned methods, there is a lack of purification steps for the synt...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C51/41C07C51/42C07C51/43C07C51/47C07C51/487C07C53/06B01D9/02
CPCC07C51/41C07C51/42C07C51/43C07C51/47C07C51/487B01D9/0013B01D9/0031C07C53/06
Inventor 张卫刚张满仓许风云杜郭社张卫军
Owner 阳城县正达新型材料股份有限公司
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