Anodic oxygenation method and operation apparatus thereof
A technology of anodizing and anodizing film, applied in anodizing, chemical instruments and methods, transportation and packaging, etc., can solve problems such as unsatisfactory, weakened oxidizing ability, and increased surface resistance of metal bodies.
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Embodiment 1
[0146] A device of the type shown in Figures 1-3 is used. The size and volume of each sub-device are as follows:
[0147] (1) Anodizing tank:
[0148] The trough used was made of heat-resistant polyvinyl chloride and had a width of 500 mm, a length of 750 mm and a height of 550 mm.
[0149] (2) Vibration flow stirring device
[0150] An ultra-vibrating α3-type stirrer, manufactured by Nippon Techno Co., Ltd., was used.
[0151] Vibration generator: URAS VIBRATOR KEE 3.5-2B, provided by YASKAWA Co., Ltd., 250W×200V×3 phase, controlled by inverter (0.4kW)
[0152] Vibrating vane: effective area 300×100mm, thickness 0.5mm (use 5 vibrating vanes), α=15 degrees (the lowest vane is inclined downward, and the other vanes are inclined upward)
[0153] Blade amplitude: 1.5mm
[0154] (3) Diffusion tube:
[0155] The MICRO AERATOR BM-100 used is made of ceramics and manufactured by Nippon Techno Co., Ltd.
[0156] Inner diameter: 50mm
[0157] Outer diameter: 75mm
[0158] Leng...
Embodiment 2
[0222] The anodizing process was carried out under the same conditions as in Example 1, except that the vibration motor output power of the device (A) was 150V, the anode potential was 15V, and the treatment liquid temperature was 30°C, and the treatment time was 5 minutes. The results are shown in Table 3.
Embodiment 3
[0239] The anodizing process was carried out under the same conditions as in Example 1, except that the aluminum plate of the processing target was changed to a duralumin plate made of A5052P (JIS H400).
[0240] Si = 0.25% or less
[0241] Fe = 0.04% or less
[0242] Cu=0.01%
[0243] Mn = 0.01 or less
[0244] Mg=2.2-2.8%
[0245] Cr=0.15-0.35%
[0246] Zn = 0.1 or less
[0247] The results are shown in Table 4
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