Method for producing potassium formate
A technology of potassium formate and formic acid, applied in the direction of carboxylate preparation, organic chemistry, etc., can solve the problems of high production cost, high technical difficulty, complicated manufacturing process, etc., and achieve the effects of easy operation, simple process and low production cost
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Embodiment 1
[0011] Embodiment 1: In this embodiment, formic acid and potassium hydroxide are used as raw materials. First, solid flake potassium hydroxide is added to the reactor from the feed port of the reactor, and then the reactor cooling water circulation system is opened to control the reaction in the reactor. The temperature at time, then the metered formic acid is added in the reactor from the top of the reactor, the amount of formic acid and potassium hydroxide addition is the proportioning of its molecular weight ratio. Such as: the molecular weight ratio of formic acid and potassium hydroxide is 46:56, the content of formic acid is 85%, and the content of potassium hydroxide is 94%, then the addition amount of formic acid and potassium hydroxide is 1:1.1, that is, add Content is 1.1 tons of potassium hydroxide of 94%, proportioning adding content is 1 ton of formic acid of 85%, after adding formic acid, start the stirrer of reactor, adjust the flow of cooling water, control the ...
Embodiment 2
[0012] Embodiment 2: present embodiment is that formic acid and salt of wormwood are main raw materials to produce potassium formate, and its technical process is basically the same as embodiment 1, because the molecular weight ratio of formic acid and salt of wormwood is 92: 138; Its content of the formic acid of use is 85%, and the addition amount is 1 ton; the content of potassium carbonate is 98%, and the addition amount is 1.3; first, potassium carbonate is added to the reactor from the feeding port of the reactor, and the cooling water circulation system is opened, and then formic acid is added from the top of the reactor. , start the agitator, adjust the flow of cooling water, control the reaction temperature in the reactor to be 50 ± 2 ° C, open the reactor pressure control valve, make the pressure in the reactor be normal pressure, after the reaction is completed to prepare potassium formate, put Potassium formate is sent into the evaporator, the temperature inside the...
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