Method for producing cigarette spicery made from extractive material of tobacco as raw material
A technology for tobacco extract and tobacco flavor, which is applied in the directions of essential oils/flavors, fat generation, etc., can solve the problems of time-consuming, no choice, lengthy process routes, etc.
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Embodiment 1
[0024]Weigh 450g of oriental tobacco extract, add 100g of water in the container, stir into a uniform tobacco extract slurry, dissolve 50g of alanine, 45g of maltose, 1g of furanone, and 2g of dihydroxyacetone in the container with 300g of water to form a solution. Pour the above-mentioned slurry and solution into the autoclave, then rinse the remaining slurry and solution in the container with 100g of water, then pour it into the autoclave, then add 3000g of propylene glycol and stir to form a uniform reaction system, adjust the reaction with concentrated ammonia water The pH of the material system is 8, and the high-pressure reactor is sealed well, and the temperature is increased under stirring, and the stirring rate is 200 rpm. When the temperature rises to 150°C, the pressure of the reactor is adjusted to 2MPa with nitrogen or carbon dioxide, and then React under constant pressure (150°C, 2MPa) for 2 hours. After the reaction, pass water to cool down to below 30°C, and st...
Embodiment 2
[0026] Weigh 500 g of water to dissolve 50 g of glutamic acid, 15 g of glycine, 50 g of glucose and 350 g of Yunyan extract. After dissolving, glucose and amino acid are added in the autoclave, then add 2000g propylene glycol, adjust the pH of the reaction system with acetic acid to be 5, seal the autoclave, turn on the electricity to heat up, and stir at the same time, the stirring speed is 300rpm, when the temperature rises to After 140°C, adjust the reaction pressure to 1.0 MPa, and react at constant temperature and pressure for 4 hours. After the reaction is finished, pass water to cool down to 25°C. The samples were stored in the reaction kettle overnight, which was beneficial to the further alcoholization of the samples. Filter with double-layer gauze to filter out the insoluble matter, and the obtained filtrate is the product of the present invention-flavor for tobacco. Seal in a plastic bottle and store in a refrigerator at 4°C. The obtained flavor for tobacco has b...
Embodiment 3
[0028] Weigh 300g Yunyan extract, 31g glucose, 2g dihydroxyacetone, 1g ascorbic acid, 10g alanine, 8.5g aspartic acid, 3.5g proline, 6.5g glutamic acid and 5g tyrosine. Add 200g of water to the Yunyan extract placed in the container, stir to form a uniform slurry, put 800g of water in the container to dissolve all amino acids, glucose, dihydroxyacetone, etc., and stir to form a uniform solution, mix the above slurry and solution Pour into a high-pressure reactor, rinse the remaining slurry and solution in the container with 100g of water, pour it into a high-pressure reactor, then add 2500g of glycerol, stir to form a uniform reaction system, and adjust the pH of the reaction system with concentrated ammonia water =7.0, seal the high-pressure reactor well, heat it up with electricity under stirring, the stirring rate is 300 rpm, when the temperature rises to 160°C, adjust the pressure of the reactor to 2MPa with nitrogen or carbon dioxide, and (160°C, 2MPa) to react for 1 hour...
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