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Method for producing cigarette spicery made from extractive material of tobacco as raw material

A technology for tobacco extract and tobacco flavor, which is applied in the directions of essential oils/flavors, fat generation, etc., can solve the problems of time-consuming, no choice, lengthy process routes, etc.

Inactive Publication Date: 2003-05-07
YINGTAN HUABAO FLAVORS & FRAGRANCES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The domestic production of individual amino acids still needs to rely on imports, that is, to rely on foreign methods to produce spices. Not only is there a limited variety of spices to choose from, but also the aroma of the resulting spices is not realistic and natural, and the quality of tobacco smoking is also quite limited; U.S. Patent (3,920,026) discloses a "tobacco flavoring agent", which mainly utilizes carbonyl compounds such as valine and dihydroxyacetone or pyruvic acid to prepare tobacco flavoring agents, but there are also aromas that are not realistic and natural. Tobacco quality improvement is also limited. In addition, the variety is relatively single, and there is no room for choice; Chinese patent (CN1039776C) discloses "a method for preparing tobacco spices". It can be seen that the process route of this method is lengthy, complicated, and time-consuming, and the carbonyl ammonia reaction is carried out under normal pressure in an open container. Many low-boiling spice components, It has escaped from the reaction system for a long time and does not participate in the carbonyl ammonia reaction, so the fragrance finally obtained by this method only contains more than 20 low-boiling components (see the records in lines 5-8 on page 3 of the patent authorization announcement), which makes the fragrance inferior. few
[0003] In a word, so far, there are still relatively few types of tobacco flavorings disclosed, and there is not much room for choice, which hinders the further development of the tobacco industry to a certain extent. For this reason, the industry department hopes that relevant scientific and technological personnel can provide a price Inexpensive, simple and easy method for preparing tobacco flavors, and can produce a wide variety of tobacco flavors, so as to promote the technological progress of the tobacco industry

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024]Weigh 450g of oriental tobacco extract, add 100g of water in the container, stir into a uniform tobacco extract slurry, dissolve 50g of alanine, 45g of maltose, 1g of furanone, and 2g of dihydroxyacetone in the container with 300g of water to form a solution. Pour the above-mentioned slurry and solution into the autoclave, then rinse the remaining slurry and solution in the container with 100g of water, then pour it into the autoclave, then add 3000g of propylene glycol and stir to form a uniform reaction system, adjust the reaction with concentrated ammonia water The pH of the material system is 8, and the high-pressure reactor is sealed well, and the temperature is increased under stirring, and the stirring rate is 200 rpm. When the temperature rises to 150°C, the pressure of the reactor is adjusted to 2MPa with nitrogen or carbon dioxide, and then React under constant pressure (150°C, 2MPa) for 2 hours. After the reaction, pass water to cool down to below 30°C, and st...

Embodiment 2

[0026] Weigh 500 g of water to dissolve 50 g of glutamic acid, 15 g of glycine, 50 g of glucose and 350 g of Yunyan extract. After dissolving, glucose and amino acid are added in the autoclave, then add 2000g propylene glycol, adjust the pH of the reaction system with acetic acid to be 5, seal the autoclave, turn on the electricity to heat up, and stir at the same time, the stirring speed is 300rpm, when the temperature rises to After 140°C, adjust the reaction pressure to 1.0 MPa, and react at constant temperature and pressure for 4 hours. After the reaction is finished, pass water to cool down to 25°C. The samples were stored in the reaction kettle overnight, which was beneficial to the further alcoholization of the samples. Filter with double-layer gauze to filter out the insoluble matter, and the obtained filtrate is the product of the present invention-flavor for tobacco. Seal in a plastic bottle and store in a refrigerator at 4°C. The obtained flavor for tobacco has b...

Embodiment 3

[0028] Weigh 300g Yunyan extract, 31g glucose, 2g dihydroxyacetone, 1g ascorbic acid, 10g alanine, 8.5g aspartic acid, 3.5g proline, 6.5g glutamic acid and 5g tyrosine. Add 200g of water to the Yunyan extract placed in the container, stir to form a uniform slurry, put 800g of water in the container to dissolve all amino acids, glucose, dihydroxyacetone, etc., and stir to form a uniform solution, mix the above slurry and solution Pour into a high-pressure reactor, rinse the remaining slurry and solution in the container with 100g of water, pour it into a high-pressure reactor, then add 2500g of glycerol, stir to form a uniform reaction system, and adjust the pH of the reaction system with concentrated ammonia water =7.0, seal the high-pressure reactor well, heat it up with electricity under stirring, the stirring rate is 300 rpm, when the temperature rises to 160°C, adjust the pressure of the reactor to 2MPa with nitrogen or carbon dioxide, and (160°C, 2MPa) to react for 1 hour...

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PUM

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Abstract

A process for preparing the perfume of cigarette from tobacco extract includes such steps as mixing it with one or omre amino acids, or amino compounds, saccharide or its compound, water and solvent, regulating pH value to 4-10, heating while pressurizing, and reaction. Its advantages are low cost and high quality of fragrance.

Description

technical field [0001] The invention relates to a preparation method of spices, in particular to a production method of tobacco spices. Background technique [0002] At present, most of the tobacco flavors added to tobacco in my country are prepared by traditional blending methods, that is, blending with various natural flavors and synthetic compounds. Although the process of the spices prepared by the compounding method is relatively simple, due to the limitation of the raw materials, the aroma of the spices obtained is monotonous, the aroma is not realistic, and the improvement of tobacco is poor. Therefore, my country's tobacco industry is in a relatively backward state. Though a kind of Maillard reaction is disclosed abroad to prepare the method for tobacco spices, owing to stay in the research that utilizes a small number of one or two simple amino acids and glucose reaction, generate Maillard reaction product, so product variety is less, ...

Claims

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Application Information

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IPC IPC(8): C11B9/00
Inventor 罗昌荣刘涵刚孙旭波
Owner YINGTAN HUABAO FLAVORS & FRAGRANCES
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