Cinnamon twig and poria soft capsule and its preparation method
A technology of cinnamon twigs and soft capsules, which can be used in capsule delivery, pharmaceutical formulations, medical preparations containing active ingredients, etc. It can solve the problems of hard capsules, such as bad smell, slow drug dissolution rate, and slow absorption by the human body, to prevent Dispersion of bitter taste and bad smell, easy control of loading difference, not easy to oxidize and volatilize
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Embodiment 1
[0029] [embodiment 1] ethanol extraction
[0030] 1.1 The influence of the fragmentation degree of medicinal materials on the extraction
[0031] Take cinnamon twigs, peach kernels, white peony root, peony cortex and poria cocos according to the prescription and break them into particles of different particle sizes, extract them according to the extraction process of cinnamon twigs and poria cocos capsules, and investigate the ointment rate of alcohol extraction, water extraction ointment rate, and alcohol extraction liquid The content of paeonol, the content of paeoniflorin in the alcohol extract, and the content of paeoniflorin in the water extract.
[0032] try
test
No
break
broken
Spend
alcohol extract
Creaming rate
water extract
Creaming rate
Alcohol Extraction Zhongdan
(g)
Peony in Alcohol Extract
Glycoside content (g)
Paeoniae officinalis in w...
Embodiment 2
[0038] [embodiment 2] the concentration of alcohol extract
[0039] Take the alcohol extracts and concentrate them at 60°C, 80°C, 100°C and normal pressure to the liquid extracts with a relative density of 1.25 (50°C), respectively measure the paeonol content in each liquid extract, and then draw the Yield of paeonol in concentrated liquid extract. The experimental results are shown in Table 4.
[0040] sample number
[0041] As can be seen from the above table, when the concentration temperature is controlled below 80°C, the yield of paeonol is about 70%, which is the preferred solution of the present invention.
Embodiment 3
[0042] [embodiment 3] water extraction
[0043] Taking the number of extractions, the amount of water added, and the extraction time as the investigation factors, using the ointment yield and the content of paeoniflorin in the extract as the investigation index, the experiment was carried out according to the L9(3)4 orthogonal experiment table, and the water extraction was determined according to the analysis of the experimental results. craft. For the factor levels of its orthogonal experiment, see
[0044] Level
[0045] The test results show that: with the ointment yield as the index, the factor C has the greatest influence, and the factor A has the least influence, and the best process is A2B3C3; taking the paeoniflorin content as the index, the factor C has the greatest influence, and the factor A has the least influence.
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