Novel ring-shape small-peptide BA and its use
A cyclic, molecular weight technology, applied in the field of biomedicine, can solve the problems of high cost, easy degradation, short half-life, etc., and achieve the effects of simple structure, strong activity and convenient artificial synthesis.
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[0027] The substantive content of the present invention is further described below with embodiment, but content of the present invention is not limited thereto.
[0028] The amino acid sequence of the cyclic small peptide BA is:
[0029] Cys Trp Thr Lys Ser Ile Pro Pro Lys Pro Cys
[0030] 5 10
[0031] Preparation of cyclic small peptide BA and its transformation method as a template:
[0032] I. The preparation method of the cyclic small peptide BA: Synthesize its complete sequence with an automatic peptide synthesizer. Reversed phase C by HPLC 18 Column desalting and purification.
[0033] II. Molecular weight determination adopts fast atom bombardment mass spectrometry (Fast atom bombardment massspectrometry, FAB-MS), with glycerol: m-nitrobenzyl alcohol: dimethyl sulfoxide (1:1:I, V:V:V, volume ratio) as substrate, Cs + As the bombardment particles, the current is 1μA and the emission voltage is 25Kv.
[0034] III. The purity of the cyclic small ...
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