Wool fiber modification treatment method
A wool fiber and wool technology, which is applied in the processing field of modified wool fiber, can solve problems such as limited friction, disordered tops, impact, etc., and achieve soft and smooth hand feeling, improved dimensional stability, and excellent luster.
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Embodiment 1
[0021]For undyed wool fibers, the modification process is: wool fiber → pre-oxidation treatment → washing → oxidation treatment → washing → reduction treatment → washing → enzyme hydrolysis treatment → washing → (dyeing → washing) → softening treatment → centrifugal dehydration → drying → modified wool fiber.
[0022] Wool loose fiber: Put 100Kg of loose fiber into the intermittent wool dyeing machine, add 3Kg of sodium percarbonate and 0.9Kg of tetraacetylethylenediamine at 30-32°C, run for 30 minutes, turn on the water, and then use 30-32°C Wash with water for 10 minutes and drain the water. Then, add 0.8Kg high-efficiency penetrant SP-2 and 5Kg ammonium persulfate at 28-30°C, run for 25 minutes, drain water, wash with water at 30-32°C for 10 minutes, and drain water. Next, add 5Kg of sodium metabisulfite at 38-40°C and run for 20 minutes, drain water, and wash with water at 30-32°C for 10 minutes. Continue to heat up to 52-53°C, add 0.8Kg alkaline protease and a certain a...
Embodiment 2
[0024] Wool loose fiber: put 100Kg loose fiber into the intermittent wool dyeing machine, add 5Kg sodium percarbonate and 2.5Kg tetraacetylethylenediamine at 30-32°C, run for 30 minutes, drain water, and then use 30-32°C Wash with water for 10 minutes and drain the water. Then, at 28-30°C, add 0.5Kg of high-efficiency penetrant SP-2 and 4Kg of a mixture of ammonium persulfate and sodium persulfate with a mass ratio of 1:1, run for 30 minutes, drain water, and then use 30-32°C water Wash for 10 minutes and turn on the water. Next, add 4Kg of a mixture of sodium metabisulfite and sodium sulfite with a mass ratio of 1:1 at 38-40°C, run for 25 minutes, drain water, and wash with water at 30-32°C for 10 minutes. Continue to heat up to 52-53°C, add 0.8Kg alkaline protease and a certain amount of soda ash, use pH test paper to test the pH value of the solution to 7.8, run for 25 minutes, continue to heat up to 75°C, run for 10 minutes, turn on the water, and then use 30 Wash in -32...
Embodiment 3
[0026] Wool loose fiber: After enzymatic hydrolysis treatment, wool loose fiber can be dyed with conventional acid dyes, neutral dyes or reactive dyes in intermittent loose wool dyeing machines, and finally softened, dehydrated and dried. The processing conditions relevant to the present invention are the same as in Example 1. It can be used to produce dyed wool modified loose fiber.
[0027] In the technical solution of the present invention, wool dyeing is to use acid dyes, neutral dyes, reactive dyes, cationic dyes, basic dyes, and disperse dyes to prepare dyed wool fibers, wool / acrylic fibers and wool / polyester fibers with conventional dyeing methods.
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