Method for refining lipid
A refining method and oil technology, applied in the direction of edible oil/fat, food science, application, etc., can solve the problems of inability to effectively eliminate or reduce membrane pollution, restore membrane flux, inability to completely remove dirt, long cleaning time, etc. Achieve the effect of less emission, high degree of flux recovery and easy cleaning
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Embodiment 1
[0047] Example 1 Refined rapeseed mixed oil
[0048] First step, membrane degumming
[0049] Rapeseed mixed oil (oil content 21.5%) is filtered by plate and frame to remove solid impurities, and then degummed and decolorized through a dead-end filter assembly (membrane MPS-U20-S, filtration temperature 35°C, maintaining working pressure 0.1-0.9MPa) for 25 hours; Wash the ultrafiltration membrane with 1wt% enzyme preparation I (50wt% Candida antarctica lipase, 49wt% porcine pancreas phospholipase A and 1wt% subtilisin) aqueous solution at 45°C for 15min, and wash the ultrafiltration membrane with warm water (45°C) After 10 minutes, the membrane was reused.
[0050] The second step, deacidification by nanofiltration
[0051] Degumming-decolorization mixed oil passes through nanofiltration membrane (membrane NTGS-2200, maintains working pressure 0.1-0.8MPa, temperature 35°C) and operates for 55h; Wash the ultrafiltration membrane for 10 minutes, wash the ultrafiltration membra...
Embodiment 2
[0054] Example 2 Refined soybean mixed oil
[0055] First step, membrane degumming
[0056] Soybean mixed oil (oil content 20.5%) is filtered by plate and frame to remove solid impurities, and degummed-decolorized by cross-flow filter module (membrane MF-50, filtration temperature 40°C, maintaining working pressure 0.1-0.8MPa), concentration ratio (initial Volume / (initial volume of feed liquid-membrane permeate volume)) 8, operation 20h; With 1wt% enzyme preparation I (55.0wt% porcine pancreatic lipase, 44.5wt% streptococcal phospholipase A and 0.5wt% papain) Wash the ultrafiltration membrane with aqueous solution at 40°C for 20 minutes, wash the ultrafiltration membrane with warm water (40°C) for 10 minutes, and reuse the membrane.
[0057] The second step, deacidification by nanofiltration
[0058] The degummed-decolorized mixed oil is passed through a nanofiltration membrane (FilmTec BW30 membrane, maintained at a working pressure of 0.1-0.7 MPa, at a temperature of 40°C)...
Embodiment 3
[0061] Example 3 Refining machine pressed sunflower oil
[0062] First step, membrane degumming
[0063] Machine-pressed sunflower oil plate and frame filter to remove solid impurities, pass through a cross-flow filter module (membrane MPS-U20S, filter temperature 30 ℃, maintain working pressure 0.1~0.9MPa) degumming-decolorization, concentration ratio 6, operate 20h; With 1wt% enzyme preparation I (60wt% porcine pancreatic lipase, 39wt% Aspergillus oryzae phospholipase A and 1 wt% trypsin) aqueous solution at 45° C. to wash the ultrafiltration membrane for 15 minutes, warm water (45° C.) to wash the ultrafiltration membrane for 8 minutes, and then use the membrane again.
[0064] The second step, deacidification by nanofiltration
[0065] Degumming-decolorizing oil is dissolved in ethanol (oil / alcohol, 4:1, w / v), passes through nanofiltration membrane (membrane NFM2221, maintains working pressure 0.1-0.8MPa, temperature 35°C), operates for 45h; with 0.5wt% enzyme Preparat...
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