Micro-encapsulated broad spectrum pollution-free fertilizer with pesticide, preparation method and application thereof

A technology of microencapsulation and fertilizer, applied in the directions of botanical equipment and methods, application, fertilizer form, etc., can solve the problems of no shielding function, complex production process, high use cost, slow down the release and decomposition speed, save energy Labor cost, the effect of not polluting the environment

Inactive Publication Date: 2009-08-26
YUXI SHANSHUI BIOSCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The above technical products have the following defects and deficiencies: they have no shielding function, cannot effectively solve the chemical compatibility and physical stability of the medicinal fertilizer preparation in the same system, and cannot solve the problem of photolysis and The problem of hydrolysis cannot solve the problem of pesticide a

Method used

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  • Micro-encapsulated broad spectrum pollution-free fertilizer with pesticide, preparation method and application thereof
  • Micro-encapsulated broad spectrum pollution-free fertilizer with pesticide, preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0021] Example 1

[0022] Put the abamectin into the reactor and fully dissolve the turpentine, add toluene diisocyanate and Tween and mix well, then pump the mixed solution to the shear emulsification reaction with ammonia water to adjust the pH of the water to 8 In the kettle, under the condition of 30℃, shear emulsification reaction for 30 minutes. After encapsulation, pesticide microcapsules are prepared; put the prepared pesticide microcapsules into the mixer, add the aqueous amino acid solution, and mix well. , Prepared microencapsulated broad-spectrum pollution-free fertilizer.

[0023] The raw materials and weight ratio of the prepared pesticide microcapsules are:

[0024] Abamectin 10 parts

[0025] 10 parts turpentine

[0026] Toluene diisocyanate 1 part

[0027] Tween 10 servings

[0028] The raw materials and weight ratio of the prepared microencapsulated broad-spectrum pollution-free fertilizer are:

[0029] Pesticide microcapsule 1 serving

[0030] 90 parts of amino ...

Example Embodiment

[0047] Example 2

[0048] Put pyrethrins and matrine into the reaction kettle, dissolve them with eucalyptus oil and cyclohexanone, add hexamethylene diisocyanate, terephthaloyl chloride, phthaloyl chloride, and Tween and mix well. The mixed solution is pumped to a shear emulsification reactor equipped with ammonia water to adjust the pH of the water to 10, at a temperature of 60 ℃, shear emulsification reaction for 120 minutes, after encapsulation, the pesticide micro Capsule: Put the prepared pesticide microcapsules into the mixer, add the amino acid aqueous solution, fully stir and mix evenly, to prepare the microencapsulated broad-spectrum pollution-free fertilizer.

[0049] The raw materials and weight ratio of the prepared pesticide microcapsules are:

[0050] Pyrethrin 45 parts

[0051] 20 parts of matrine

[0052] Eucalyptus oil 10 parts

[0053] 55 parts of cyclohexanone

[0054] 1 part of hexamethylene diisocyanate

[0055] Terephthaloyl chloride 1 part

[0056] Phthaloy...

Example Embodiment

[0084] Example 3

[0085] Put abamectin, pyrethrin, and matrine into the reaction kettle and dissolve them with turpentine oil, eucalyptus oil, and cyclohexanone. Add toluene diisocyanate, hexamethylene diisocyanate, terephthaloyl chloride, The phthaloyl chloride and Tween are mixed uniformly, and the mixed solution is pumped to the shear emulsification reactor equipped with ammonia water to adjust the pH of the water to 9. Under the condition of 50 ℃, the shear emulsification reaction After 90 minutes, after encapsulation, the pesticide microcapsules are prepared; the prepared pesticide microcapsules are put into the mixer, the organic fertilizer is added, and the mixture is fully stirred and mixed to obtain the microencapsulated broad-spectrum pollution-free pesticide fertilizer.

[0086] The raw materials and weight ratio of the prepared pesticide microcapsules are:

[0087] Abamectin 5 parts

[0088] Pyrethrin 5 parts

[0089] Matrine 10 servings

[0090] Turpentine 20 parts

...

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Abstract

The invention discloses a micro-encapsulated broad spectrum pollution-free fertilizer with pesticide, a preparation method and application thereof. The fertilizer with pesticide consists of 1 to 10 portions of pesticide microcapsule and 90 to 99 portions of nutrient substances in portion by weight. The preparation method thereof mainly comprises the following steps: filling the pesticide into a reaction kettle and thoroughly dissolving the pesticide by a solvent, adding wall material monomer and Tween into the kettle respectively, evenly mixing the solution, conveying the mixed solution to a shear emulsion reaction kettle by a pump to carry out shear emulsion reaction, and forming capsules to obtain the pesticide microcapsule; and adding the nutrient substances into the pesticide microcapsule, fully stirring and evenly mixing the mixture to obtain the natural product micro-encapsulated broad spectrum pollution-free fertilizer with pesticide. The chemical compatibility and physical stability problem of the prior pesticide fertilizer preparation in a same system can be effectively solved by using the method. The product has the advantages that the fertilizer with pesticide has shielding and slow-release functions, the chemical compatibility and physical stability are good, the drug effect is durable, the using cost is low, and the production process is simple.

Description

technical field [0001] The invention relates to a non-public drug fertilizer, in particular to a high-efficiency, low-cost microencapsulated broad-spectrum pollution-free drug fertilizer and its preparation method and application. Background technique [0002] Japan began to mix the herbicide pentachlorophenol (pcp) into fertilizers as a base fertilizer in the 1960s, in order to achieve the purpose of saving manpower and continuing the weeding effect. In the mid-1960s, the United States found that procyon can strongly inhibit nitrification and denitrification, reduce nitrogen loss, and can also enhance biological nitrogen fixation, increase nitrogen content in soil, and effectively enhance fertilizer efficiency. The mixed application of nitrogen, phosphorus, potassium fertilizer and 2,4-d in corn production also showed obvious synergistic effect on weeding and yield. In the early 1980s, the United States proposed more than 300 kinds of herbicides and 5 kinds of compound fer...

Claims

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Application Information

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IPC IPC(8): C05G3/00C05G5/00C05G3/02A01N43/90A01N53/10A01P7/04C05G3/60
Inventor 蒲恩堂罗波孔宁川侯金荣
Owner YUXI SHANSHUI BIOSCI
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