Microporous aluminum oxide burning plate and preparation method thereof
A technology of alumina and setter, applied in the field of refractory material preparation and ceramics, can solve the problem of inability to prepare high-purity, microporous alumina setter, unable to meet the requirements of high-purity, porous alumina setter, and the inability of the production process. It can meet the problems of preparing microporous materials, and achieve the effect of ensuring the uniformity of pores, promoting sintering, and reducing the sintering temperature.
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Embodiment 1
[0025] The raw material components and the mass percentage of each component are: 80% of α-alumina with a particle size of less than 1um, 3% of polyacrylamide, 15% of boehmite, and 2% of hexamethylphosphoric triamide.;
[0026] Its process steps are as follows:
[0027] 1) Add α-alumina, polyacrylamide and boehmite into the polyurethane mixing tank in proportion and add water to make a slurry with a solid content of 60% and blend for 5 hours;
[0028] 2) Add hexamethylphosphoric triamide to the slurry mixed in step 1 and stir for 30 minutes with a high-speed mixer (1000 rpm);
[0029] 3) Inject the slurry prepared in step 2 into a plastic mold, scrape the upper surface of the slurry, put it into an environment with a temperature of 40 degrees and a temperature of 70%, and maintain it for 10 hours to fully solidify;
[0030] 4) demoulding the solidified green body and putting it into an oven at 110°C to fully dry it;
[0031] 5) Put the dried green body into an electric furna...
Embodiment 2
[0036] The raw material components and the mass percentage of each component are: 85% of α-alumina with a particle size of less than 1um, 4% of polyacrylamide, 10% of boehmite, and 1% of hexamethylphosphoric triamide;
[0037] Its process steps are as follows:
[0038] 1) Add α-alumina, water-based resin polyacrylamide, and boehmite into the mixing tank according to the proportion, and add water to make a slurry with a solid content of 60% and blend for 3 hours;
[0039] 2) Add hexamethylphosphoric triamide to the slurry mixed in step 1 and stir with a high-speed mixer for 30 minutes;
[0040] 3) Inject the slurry prepared in step 2 into a plastic mold, scrape the upper surface of the slurry, put it into an environment with a temperature of 40 degrees and a temperature of 70%, and maintain it for 10 hours to fully solidify;
[0041] 4) demoulding the solidified green body and putting it into an oven at 110°C to fully dry it;
[0042] 5) Put the dried green body into an elect...
Embodiment 3
[0046] The raw material components and the mass percentage of each component are: 82% of α-alumina with a particle size of less than 1um, 5% of polyacrylamide, 11.5% of boehmite, and 1.5% of hexamethylphosphoric triamide.;
[0047] Its process steps are as follows:
[0048]1) Add alumina, water-based resin polyacrylamide, and boehmite to the mixing tank according to the proportion, and add water to make a slurry with a solid content of 60% and blend for 5 hours;
[0049] 2) Add hexamethylphosphoric triamide to the slurry mixed in step 1 and stir with a high-speed mixer for 30 minutes;
[0050] 3) Inject the slurry prepared in step 2 into a plastic mold, scrape the upper surface of the slurry, put it into an environment with a temperature of 40 degrees and a temperature of 70%, and maintain it for 10 hours to fully solidify;
[0051] 4) demoulding the solidified green body and putting it into an oven at 110°C to fully dry it;
[0052] 5) Put the dried green body into an elect...
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