Acid scouring agent and preparation method thereof

A soaping agent and acid technology, which is applied in the field of soaping after dyeing of cellulose fibers and its preparation field, can solve the problem of lack of residual alkali, and achieve the effects of reducing the number of washings, high chelation value, and improving work efficiency.

Active Publication Date: 2010-06-16
苏州联胜化学有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In recent years, polymer copolymer type soaping agents have had certain research and development, such as the anti-contamination cleaning agents studied by Wang Xiangrong, Pu Zongyao, etc. The high molecular copolymerization is a sodium salt type, which is neutral or weakly alkaline, and does not have the ability to neutralize the residual alkali on the cloth surface

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] 1. Preparation of copolymer:

[0042] A, the preparation of initiator aqueous solution: 10 kilograms of ammonium persulfates are added water 90 kilograms and are made initiator aqueous solution;

[0043] B. Synthesis of copolymer: In a 1-ton enamel reaction kettle, add 305 kg of water, 22 kg of maleic acid, 10.6 kg of fumaric acid, 20.5 kg of acrylamide and 24 kg of acrylic acid, heat up to 50-70 ° C, add 24 kg of sodium bisulfate and 30 kg of ammonium persulfate aqueous solution, the solution is automatically heated to 70-90 ° C, maintain the temperature, slowly add 96 kg of acrylic acid and the remaining ammonium persulfate aqueous solution 7, after the addition is completed, the temperature is 80-90 ℃ for 3-6 hours, then cool down to below 40 ℃.

[0044] C. Compounding of acid soaping agent for environment-friendly dyeing

[0045] Add 26 kilograms of polyvinylpyrrolidone PVP, 65 kilograms of sodium gluconate and 98 kilograms of water to the above-mentioned product,...

Embodiment 2

[0047] 1. Preparation of copolymer:

[0048] A, the preparation of initiator aqueous solution: 8.4 kilograms of ammonium persulfates are added water 76 kilograms and are made initiator aqueous solution;

[0049] B. Synthesis of copolymer: In a 1 ton enamel reaction kettle, add 240 kg of water, 16 kg of maleic acid, 5.6 kg of fumaric acid, 8.3 kg of acrylamide and 16 kg of acrylic acid, heat up to 50-70 ° C, add 21 kg of sodium bisulfate and 22 kg of ammonium persulfate aqueous solution, the solution automatically heats up to 70-90 °C, maintain the temperature, slowly add 88 kg of acrylic acid and the remaining ammonium persulfate aqueous solution, after the addition is completed, keep warm at 80-90 °C 3-6 hours, then cool down to below 40°C.

[0050] C. Compounding of acid soaping agent for environment-friendly dyeing

[0051] Add 28 kilograms of polyvinylpyrrolidone PVP, 46 kilograms of sodium gluconate and 300 kilograms of water to the above-mentioned product, stir fully t...

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PUM

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Abstract

The invention discloses an acid scouring agent and a preparation method thereof. The acid scouring agent comprises a multivariate acidic copolymer, polyvinyl pyrrolidone PVP and sodium gluconate. The scouring agent does not contain phosphorus, alkylphenol ethoxylates and harmful solvents and is degradable; and at the same time, the scouring agent has the characteristics of a little foam, high chelation value and high alkali neutralizing capacity. The scouring agent can be used for scouring cellulose fibers after dyeing, can simplify the traditional process and contributes to energy conservation and emission reduction.

Description

technical field [0001] The invention relates to a reagent for the textile dyeing and finishing industry and a preparation method thereof, in particular to a reagent for soaping after dyeing cellulose fibers and a preparation method thereof. Background technique [0002] The printing and dyeing industry is an important component of the textile industry, and it is also an industry with high energy consumption and large sewage discharge. In the printing and dyeing industry to carry out energy saving and emission reduction work, in addition to research and development of high-efficiency, water-saving, and energy-saving equipment, and the development and promotion of practical new technologies for energy-saving and water-saving, the use of high-efficiency, environmental protection, water-saving, and energy-saving dyeing and chemical materials is the most popular at this stage. It is an effective method with less investment and quick results. [0003] Reactive dyes are generally ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P5/08C08F220/06
Inventor 李安实涂胜宏
Owner 苏州联胜化学有限公司
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