Preparation method of coal dust suppressant with nuclear membrane structure
A technology of dust suppressant and coal, applied in the direction of chemical instruments and methods, other chemical processes, etc., can solve problems such as short circuit of power supply insulators, deterioration of the environment of employees and passengers, and high cost
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Embodiment 1
[0025] Take 1.5g of tetrabutyl titanate (analytical pure) and dissolve it in 6g of ethanol (analytical pure, the same below), fully dissolve; take 1.5 g of sodium carboxymethyl cellulose and dissolve it in 88ml of distilled water; then dissolve tetrabutyl titanate The solution of the ester is dripped into the sodium carboxymethyl cellulose solution at a rate of 20-30 drops / min. After the addition is completed and fully mixed, oxalic acid (20%) is added dropwise according to the acidity at this time to make The pH value of the mixed solution is 7, and after 7 hours of reaction, an environment-friendly dust suppressant with nuclear membrane structure composed of sodium carboxymethyl cellulose, titanium oxide, dibutyl oxalate, ethanol and water can be obtained.
Embodiment 2
[0027] Take 0.3g of tetrabutyl titanate (analytical pure) and dissolve it in 4g of ethanol, fully dissolve; take 1.0g of hydroxypropyl methylcellulose and dissolve it in 90ml of distilled water; then drop the solution of tetrabutyl titanate into hydroxyl In the propyl methylcellulose solution, the dropping speed is 20-30 drops / minute. After the dropping is completed and fully mixed, oxalic acid (20%) is added dropwise according to the acidity at this time, so that the pH value of the mixed solution is 6.8 After 5 hours of reaction, an environment-friendly dust suppressant with nuclear membrane structure composed of hydroxypropyl methylcellulose, titanium oxide, dibutyl oxalate, ethanol and water can be obtained.
Embodiment 3
[0029] Take 3.0g of tetrabutyl titanate (analytical pure) dissolved in 6g of ethanol, fully dissolved; take 2.0 grams of sodium carboxymethyl starch and dissolve in 87ml of distilled water; then drop the solution of tetrabutyl titanate into carboxy In the sodium methyl starch solution, after the dropwise addition is completed and fully mixed, oxalic acid (20%) is added dropwise according to the acidity at this time, so that the pH value of the mixed solution is 7.2, and after 8 hours of reaction; Sodium starch, titanium oxide, dibutyl oxalate, ethanol and water is an environment-friendly dust suppressant with nuclear membrane structure.
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