Xylose production and purification process
A xylose and process technology, applied in the refined field of xylose production, can solve the problems of high acid and alkali consumption in resin regeneration, serious environmental pollution, and large amount of ion exchange resin, so as to shorten the production cycle, simplify the process flow, and reduce production cost effect
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[0019] 1. Put 250ml of gel-type anion exchange resin 201×4 into a jacketed, Φ24×1200mm glass exchange column, and then regenerate it with 3.0% sodium hydroxide solution at a flow rate of 1400ml / h. The water is washed at a flow rate of 1400ml / h until the pH value of the outlet is 8, and the washing liquid is clarified; the xylose decolorization solution at 30°C is passed through the resin bed at a flow rate of 500ml / h, the exchange volume is 3000ml, and the pH value of the exchange liquid is 5.1.
[0020] 2. Put 150ml of gel-type cation exchange resin Ambeilite IR120 and 150ml of macroporous anion-exchange resin D301 into jacketed, Φ24×600mm glass exchange columns respectively to form positive and negative columns in series, gel-type cation-exchange resin Ambeilite IR120 is regenerated countercurrently with 5% hydrochloric acid solution at a flow rate of 480ml / h. After regeneration, wash with pure water at a flow rate of 480ml / h to pH 5, and the washing solution is clarified; ma...
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