Method for degrading nitrobenzene waste water by polyphase electrocatalytic oxidation-Fenton coupling process and reactor thereof
A catalytic oxidation, nitrobenzene technology, applied in chemical instruments and methods, oxidized water/sewage treatment, water/sewage multi-stage treatment, etc. problems, to achieve the effect of ensuring compliance with emission standards
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[0037] Implementation example 1
[0038] In terms of weight percentages, 98% of the electrode particles accounted for activated carbon and iron filings as the matrix, with 0.01% platinum oxide, 0.02% palladium oxide, 0.1% nickel oxide, 0.2% cobalt oxide, 0.3% Zinc oxides, 0.37% copper oxides and 1% manganese dioxide are solid catalysts, and activated carbon or / and iron filings and solid catalysts are fully mixed into particles with a particle size of 4-6mm. Electrodes are used as electrodes; cathode electrode plates Use graphite, anode electrode plate uses RuO 2 -IrO 2 -TiO 2 / Ti, as the feed electrode, the initial pH of nitrobenzene wastewater is 3, the distance between the plates is 6cm, the cell voltage is 30V, Fe 2+ The dosage is 1.0g / L (add 6 times), and the aeration amount is 0.8m 3 Under the condition of COD 18000mg / L and nitrobenzene content of 1300mg / L nitrobenzene wastewater treated for 90 minutes, the removal rates of COD and nitrobenzene were 93.1% and 96.5%, respectiv...
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[0040] Implementation example 2
[0041] In terms of weight percentages, activated carbon and iron filings accounting for 94% of the electrode particles are used as the matrix, 0.01% platinum oxide, 0.02% palladium oxide, 0.2% nickel oxide, 0.3% cobalt oxide, 0.47% Zinc oxide, 1% copper oxide and 4% manganese dioxide are solid catalysts, and the active carbon or / and iron filings and solid catalyst are fully mixed to form particles with a particle size of 4-6mm. The electrode is the working electrode; cathode electrode The plate is made of graphite, and the anode electrode plate is made of RuO 2 -IrO 2 -TiO 2 / Ti, as the feed electrode, the initial pH of nitrobenzene wastewater is 2, the electrode plate spacing is 4cm, the cell voltage is 20V, Fe 2+ The dosage is 0.8g / L (addition in 4 times), and the aeration amount is 0.6m 3 The rosin production wastewater with a COD of 3440mg / L was treated for 90 minutes under the condition of / h, and the removal rate of COD was 82.5%.
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[0042] Implementation example 3
[0043] In terms of weight percentage, the iron filings accounting for 96% of the electrode particles are used as the matrix, with 0.01% platinum oxide, 0.02% palladium oxide, 0.2% nickel oxide, 0.3% cobalt oxide, and 0.47% zinc oxide. Oxide, 1% copper oxide and 2% manganese dioxide are solid catalysts, and the active carbon or / and iron filings and solid catalyst are fully mixed to form a particle electrode with a particle size of 4-6mm as the working electrode; activated carbon or / Fully mix iron filings and solid catalyst into particles with a particle size of 4-6mm. The electrode is the working electrode; the cathode electrode plate is graphite, and the anode electrode plate is RuO. 2 -IrO 2 -TiO 2 / Ti, as the feed electrode, as the feed electrode, the initial pH is 4, the distance between the plates is 8cm, the cell voltage is 40V, Fe 2+ Dosing amount is 1.2g / L (addition in 5 times), aeration amount is 1.0m 3 Under the condition of COD 273000mg...
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