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Phosphatizing liquid and preparation method thereof

A preparation method and phosphating solution technology, applied in the field of phosphating treatment, can solve the problems of steam heating pipelines that do not have large enterprises, poor production batches and overall planning, exhaust gas pollution, etc., to reduce construction difficulty and protect the environment Meager, the effect of reducing labor intensity

Inactive Publication Date: 2011-01-05
景阳富
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Many small and medium-sized enterprises generally have difficult heating conditions, do not have the steam heating pipelines of large enterprises, and generally have poor production batches and overall planning. Environment, or stop production in winter!

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] Preparation of room temperature phosphating solution 500kg:

[0036] Phosphoric acid (85%) 150--180Kg; nitric acid (68%) 80--100Kg; zinc oxide (99.7%) 78--92Kg; water (added first) 70Kg; citric acid 2--3Kg; sodium fluoride 2Kg; Nickel nitrate 3--5Kg; iron nitrate 0.8-1.2Kg; copper nitrate 0.02-0.05Kg; water (added later) balance.

Embodiment 2

[0038] Prepare 100kg ultra-low temperature accelerator:

[0039] Tartaric acid 0.5-0.8kg; citric acid 0.2-0.5kg; sodium fluoroborate 2.5-3.5kg; sodium m-nitrobenzenesulfonate 1.0-2.5kg; sodium chlorate 1.5-2.0kg; sodium nitrite 35-40kg; hydrogen peroxide 3 -5Kg; ferric nitrate 0.5-0.8Kg; deionized water balance.

Embodiment 3

[0041] Prepare neutralizer 100kg:

[0042] Caustic soda (ion membrane, 99%) 20kg, sodium carbonate (industrial grade 96%) 15kg water 65kg.

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PUM

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Abstract

The invention discloses phosphatizing liquid. The phosphatizing liquid comprises the following components in percentage by weight: 7 percent of starter liquid, 0.38 to 0.4 percent of neutralizer, 0.2 to 0.6 percent of accelerator and the balance of water, wherein the starter liquid comprises the following components in percentage by weight: 30 to 36 percent of 85 percent phosphoric acid, 16 to 20 percent of 68 percent nitric acid, 15.6 to 18.4 percent of 99.7 percent zinc oxide, 0.4 to 0.6 percent of citric acid, 0.4 percent of sodium fluoride, 0.6 to 1 percent of nickel nitrate, 0.16 to 0.24 percent of ferric nitrate, 0.004 to 0.01 percent of copper nitrate and the balance of water.

Description

technical field [0001] The invention relates to the technical field of phosphating treatment, in particular to a phosphating solution and a preparation method thereof. Background technique [0002] Since the civilization era of slash-and-burn farming, the use of tools and dependence on metals have never stopped. With the rapid development of modern industry, the output of steel has become an important symbol to measure the comprehensive strength of a country. The continuous doubling of steel production and the fact that a large amount of steel is corroded has plagued generations of producers and users. Because of this, many colleges, universities, scientific research personnel and engineering technicians have invested in the battle of steel anti-corrosion, and anti-corrosion processes and technologies such as pickling, phosphating, coating, and electroplating continue to emerge. [0003] Phosphating treatment is an indispensable treatment process for steel materials before...

Claims

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Application Information

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IPC IPC(8): C23C22/17
Inventor 景阳富
Owner 景阳富
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