Dimethyl itaconate sulfonate multi-copolymer scale inhibitor and preparation method thereof
A technology of dimethyl itaconate sulfonate and dimethyl itaconate, which is applied in chemical instruments and methods, descaling and water softening, water/sludge/sewage treatment, etc., can solve the problem of single and inorganic Large addition amount, poor anti-scaling effect and other problems, to achieve the effect of simple production process, less residual monomer and good dispersion effect
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Embodiment 1
[0023] In a four-neck flask equipped with a mechanical stirrer, a constant pressure dropping funnel, and a thermometer, add 130 g of itaconic acid, 72 g of isopropanol, and 400 g of distilled water, and heat to 60 ° C to completely dissolve the itaconic acid; Dissolve 18g of sodium in 50g of distilled water, add it quickly after itaconic acid dissolves; then heat up to 90°C; dissolve 18g of sodium propylene sulfonate in 55g of distilled water, add 100g of distilled water and 15g of sodium persulfate to prepare the initiator; Add 27g of sodium hypophosphite and 15g of dimethyl itaconate to 100g of distilled water to prepare a reducing agent; Evenly drop into the beaker within 2 hours, maintain the reaction temperature at 90 ° C, after the monomer and initiator are added dropwise, continue to keep warm (insulated for 20 minutes) and react for a period of time (hereinafter referred to as "reaction time"). Stop heating, stirring, distill, recover isopropanol, control the temperatu...
Embodiment 2
[0037]In a four-necked flask equipped with a mechanical stirrer, a constant pressure dropping funnel, and a thermometer, add 150 g of itaconic acid, 72 g of isopropanol, and 400 g of distilled water, and heat to 60 ° C to completely dissolve the itaconic acid; Dissolve 8g of sodium in 50g of distilled water, add it quickly after itaconic acid dissolves; then heat up to 90°C; dissolve 8g of sodium propylene sulfonate in 55g of distilled water, add 100g of distilled water and then 8g of sodium persulfate to prepare the initiator; Add 8g of sodium hypophosphite and 8g of dimethyl itaconate to 100g of distilled water to prepare a reducing agent; Evenly drop into the beaker within 2 hours, maintain the reaction temperature at 90 ° C, after the monomer and initiator are added dropwise, continue to keep warm (insulated for 20 minutes) and react for a period of time (hereinafter referred to as "reaction time"). Stop heating, stirring, distill, recover isopropanol, control the temperat...
Embodiment 3
[0041] In a four-necked flask equipped with a mechanical stirrer, a constant pressure dropping funnel, and a thermometer, add 120 g of itaconic acid, 72 g of isopropanol, and 400 g of distilled water, and heat to 60 ° C to completely dissolve the itaconic acid; Sodium 30g is dissolved in 80g distilled water, after itaconic acid dissolves, add quickly; then heat up to 90°C; dissolve 30g sodium propylene sulfonate in 100g distilled water, add 100g distilled water and then add 18g sodium persulfate to prepare the initiator; Add 36g of sodium hypophosphite and 24g of dimethyl itaconate to 100g of distilled water to prepare a reducing agent; Evenly drop into the beaker within 2 hours, maintain the reaction temperature at 90 ° C, after the monomer and initiator are added dropwise, continue to keep warm (insulated for 20 minutes) and react for a period of time (hereinafter referred to as "reaction time"). Stop heating, stirring, distill, recover isopropanol, control the temperature a...
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