Preparation method of metal carrier Tenax coating stirring and extracting rod
A technology for extracting rods and metal rods, which is applied in the directions of alkali metal compounds, chemical instruments and methods, alkali metal oxides/hydroxides, etc., can solve the problems of high price of SBSE devices, application limitations of SBSE technology, etc., and achieve high mechanical strength. , good thermal stability
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Embodiment 1
[0031] An iron rod with a length of 25 mm and a diameter of 2 mm was selected, and its surface was pretreated with dichloromethane. Weigh 100g of epoxy resin, add xylene and stir until completely dissolved, then add 15g of pyromellitic anhydride, 15g of tertiary amine, and 20g of asbestos powder in sequence, and stir to disperse the components evenly. Coat the surface of the treated rod with a layer of high-temperature resistant epoxy resin, then dip a layer of Tenax adsorbent on the outer layer, and place the rod in an oven at 180°C for 60 minutes to cure. The prepared extraction rod was placed in a Soxhlet extractor, and refluxed with dichloromethane at 60° C. for 40 min.
[0032] The epoxy resin is a polyfunctional glycidyl type epoxy resin, which is commercially available. The Tenax sorbent is Tenax TA.
Embodiment 2
[0034] A nickel rod with a length of 25 mm and a diameter of 2 mm was selected, and its surface was pretreated with dichloromethane. Coat the surface of the treated rod with a layer of silicone resin, then dip a layer of Tenax adsorbent on the outer layer, and place the rod in an oven at 180°C for 60 minutes to cure. The prepared extraction rod was placed in a Soxhlet extractor, and refluxed with dichloromethane at 60° C. for 40 min.
Embodiment 3
[0036] A stainless steel rod with a length of 25 mm and a diameter of 2 mm was selected, and its surface was pretreated with dichloromethane. Coat the surface of the treated rod with a layer of silicone resin, and then dip a layer of 2,6-diphenylfuran porous polymer resin on the outer layer, and place the rod in an oven at 180°C for 60 minutes to cure. The prepared extraction rod was placed in a Soxhlet extractor, and refluxed with dichloromethane at 60° C. for 40 min.
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