Infrared reflexive aggregate and preparation method thereof
A technology of infrared reflection and aggregate, applied in the direction of reflection/signal coatings, chemical instruments and methods, fibrous fillers, etc., can solve the problems of increased cooling load, high heat generation in office buildings, and inability to dissipate internal heat, and achieve improved Effects of stain resistance, improvement of external wall thermal insulation performance, and excellent infrared reflection performance
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Embodiment 1
[0045] Embodiment 1, a kind of preparation method of infrared reflective aggregate, carries out following steps successively:
[0046] 1. Pretreatment of mica
[0047] 1), select the mica with an average thickness of 0.6 μm and an average particle size of 45 μm; weigh 50 g of the above-mentioned mica and add it to a three-necked flask, and then add 1000 ml of hydrochloric acid solution (mass concentration 5%) in the three-necked flask; place the three-necked flask on In a water bath (at a constant temperature of 80°C), stir and mix for 40 minutes. After filtering, wash the filter residue with deionized water until the washing liquid is neutral; obtain washed mica;
[0048] 2), after the above-mentioned washing, mica and 1000ml of phosphoric acid solution (mass concentration 5%) were put into another three-necked flask, and this three-necked flask was placed in a water bath (65° C. constant temperature), stirred for 40 minutes, and suctioned under reduced pressure. The filter ...
Embodiment 2
[0058] Embodiment 2, a kind of preparation method of infrared reflective aggregate, carries out following steps successively:
[0059] 1. Mica pretreatment:
[0060] With embodiment 1.
[0061] 2. Preparation of doped zinc oxide-coated mica infrared reflective aggregate by homogeneous precipitation method:
[0062] 1), the ZnSO 4 、Al 2 (SO 4 ) 3 and formamide were prepared into aqueous solutions with a concentration of 0.2, 0.035, and 0.25mol / L respectively, and the above three aqueous solutions were mixed according to a volume ratio of 10:0.75:1.25, and then diluted with deionized water by one time; a mixed solution was obtained;
[0063] 2) Pour 250ml of the mixed solution into a three-necked flask, and add 5g of pretreated mica into the three-necked flask; heat up to 80° C. for 2.5 hours for hydrolysis under continuous stirring. The obtained hydrolysis reaction product was filtered under reduced pressure, washed three times, and dried to obtain a powder;
[0064] 3) ...
Embodiment 3
[0070] Embodiment 3, a preparation method of infrared reflective aggregate, the following steps are carried out in sequence:
[0071] 1. Mica pretreatment:
[0072] With embodiment 1.
[0073] 2. Preparation of doped ZnO-coated mica infrared reflective aggregate by sol-gel method
[0074] 1), take 0.2molZn(CH 3 COO) 2 2H 2 O with 0.004molAlCl 3 ·6H 2 O, placed in a three-necked flask. Get the ethylene glycol methyl ether of 256.37g and the ethanolamine (MEA) of 12.22g and add in the there-necked flask, stir and mix, thus be formulated to contain 0.75M Zn 2+ A mixed solution of ions. While stirring, the temperature was raised to 60° C., and stirred for 1 h to obtain a homogeneous AZO colloidal solution.
[0075] 2), take the above-mentioned 250ml homogeneous AZO colloidal solution, add 12g of pretreated mica, and slowly add deionized water diluted with ethylene glycol methyl ether (dilute ethylene glycol methyl ether and deionized water at a ratio of 19:1 The volume r...
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