Modified nano aluminium hydroxide water expansion type overcoating fire retardant paint and preparation method thereof

A technology of nano-aluminum hydroxide and fireproof coatings, applied in fireproof coatings, coatings, etc., can solve the problems of low flame retardant efficiency, poor fire protection effect, low raw material utilization rate, etc., and achieve good flame retardant effect and flame retardant effect Obvious, good economic effect

Inactive Publication Date: 2013-02-20
SHENYANG JIANZHU UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, their common disadvantage is that nano-inorganic substances do not undergo decomposition and endothermic reactions under high temperature, and have the defect of low flame retardant efficiency, so the utilization rate of raw materials is low, and the fire protection effect is poor.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] (A) Preparation of modified nano aluminum hydroxide powder: according to the formula, take 50 Kg of nano aluminum hydroxide powder, 2 Kg of sodium hexametaphosphate powder, and 16 Kg of water. First put the nano aluminum hydroxide powder in a beaker. Add water to prepare a slurry; place the slurry in a constant temperature water bath at 80°C-100°C; add sodium hexametaphosphate and stir well for 20-30 minutes to prepare a nano aluminum hydroxide suspension; (b), preparation additives :According to the formula ratio, first take 3 Kg of dispersant (polyacrylic acid copolymer solution), wetting agent (polyethoxy compound), and defoamer (polysiloxane) according to 1:1:1, and add 23 Kg of water, stir evenly in a mixer with a speed of 800-1700r / min for later use; (c). Mixed finished product: take the above-mentioned spare auxiliary solution, and add anatase titanium dioxide and modified nano-hydroxide according to the formula ratio The mixture of aluminum powder (modified nano ...

Embodiment 2

[0024] (A) Preparation of modified nano aluminum hydroxide powder: according to the formula, take 100 Kg of nano aluminum hydroxide powder, 0.5 Kg of sodium hexametaphosphate powder, and 25 Kg of water. First put the nano aluminum hydroxide powder in a beaker. Add water to prepare a slurry; place the slurry in a constant temperature water bath at 80°C-100°C; add sodium hexametaphosphate and stir well for 20-30 minutes to prepare a nano aluminum hydroxide suspension; (b), preparation additives : According to the formula ratio, first take the dispersant (polyacrylic acid copolymer solution), wetting agent (polyethoxy compound), and defoamer (polysiloxane) according to 1:1:1 to take 7 Kg, and add 30 Kg In the water, stir evenly at a speed of 800-1700r / min for standby; (c) Mix the finished product: take the above-mentioned standby auxiliary solution and add anatase titanium dioxide and modified nano aluminum hydroxide powder according to the formula ratio Mixture (modified nano alu...

Embodiment 3

[0026] (A) Preparation of modified nano aluminum hydroxide powder: according to the formula, take 75 Kg of nano aluminum hydroxide powder, 1.6 Kg of sodium hexametaphosphate powder, and 20Kg of water. First put the nano aluminum hydroxide powder in a beaker and add water. Prepare the slurry; place the slurry in a constant temperature water bath at 80℃-100℃; add sodium hexametaphosphate and stir well for 20-30 minutes to prepare a nano aluminum hydroxide suspension; (b), preparation additives: According to the formula ratio, first take the dispersant (polyacrylic acid copolymer solution), wetting agent (polyethoxy compound), and defoamer (polysiloxane) at 1:1:1 to take 3.5 Kg, and add 25 Kg In the water, stir evenly at a speed of 800-1700r / min for standby; (c) Mix the finished product: take the above-mentioned standby auxiliary solution and add anatase titanium dioxide and modified nano aluminum hydroxide powder according to the formula ratio Mixture (modified nano aluminum hydr...

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Abstract

The invention discloses a modified nano aluminium hydroxide water expansion type overcoating fire retardant paint and a preparation method thereof. The paint is prepared from the following raw materials in percentage by weight: 22%-28% of organic silicon modified styrene-acrylate emulsion, 13%-17% of mixture of anatase type titanium dioxide and modified nano aluminium hydroxide powder, 16%-19% of ammonium polyphosphate, 8%-13% of tripolycyanamide, 5%-9% of pentaerythritol, 3%-7% of auxiliary and 21%-27% of water; and the modified nano aluminium hydroxide is prepared from the raw materials in parts by weight: 60-85 parts of nano aluminium hydroxide powder, 0.8-2.5 parts of sodium hexametaphosphate powder and 18-24 parts of water. The paint is a water system having obvious inflaming retarding effect, high fireproof performance, good brushing resistance, weather resistance and smearing hardness and low fuming amount, and has the beneficial effects of simple production process, good dispersing effect, low cost, stable quality and long service life, and is energy-saving and environment-friendly.

Description

Technical field [0001] The invention relates to a fire retardant paint, in particular to a modified nano aluminum hydroxide water-based intumescent fire retardant paint and a preparation method thereof. Background technique [0002] The issue of fire has always attracted great attention from the Party Central Committee and the State Council. Comrade Jiang Zemin once instructed: "Hidden danger is more dangerous than open fire, prevention is better than disaster relief, and responsibility is heavier than Taishan." Relevant departments have also formulated laws and regulations on fire prevention, which will help reduce fires. As a threat to people's lives and property, fireproof coatings can effectively reduce fire losses. At present, most of the fireproof coatings developed are made by adding nano-inorganic materials with high thermal stability. For example, the invention patent "Environmentally friendly nano fireproof coatings" with the publication number: CN200810229685.1 is give...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D125/14C09D7/12C09D5/18
Inventor 赵苏杨海峰吴娇颖
Owner SHENYANG JIANZHU UNIVERSITY
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