Method for restoring stannic chloride
A technology of tin tetrachloride and tin protochloride, which is applied in the direction of tin protochloride and tin halide, can solve the problems of secondary pollution, and achieve the effects of low cost, reasonable synthesis process and environmental friendliness
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[0011] Example 1. A method for reducing tin tetrachloride, the method uses electricity as a reducing agent; the specific steps are as follows: add the use of stannous chloride to reduce diazonium in an electrolytic cell equipped with a tail gas treatment system, agitation and two metal electrodes The dilute hydrochloric acid solution of tin tetrachloride produced by the salt, stir and energize to 15A; slowly increase the temperature and react at 70°C; after detecting that there is no tetravalent tin in the solution, the reaction ends, and the dilute hydrochloric acid of stannous chloride is obtained Solution.
Example Embodiment
[0012] Example 2. A method for reducing tin tetrachloride, which uses electricity as a reducing agent; its specific steps are as follows: add it to an electrolytic cell equipped with a tail gas treatment system, stirring, a nickel electrode as the cathode, and a metal electrode with ruthenium, iridium and titanium as the anode The dilute hydrochloric acid solution of tin tetrachloride produced by the reduction of diazonium salt with stannous chloride, stir and energize to 22A; slowly increase the temperature and react at 65°C; after detecting that there is no tetravalent tin in the solution, the reaction ends, that is Obtain a dilute hydrochloric acid solution of stannous chloride.
Example Embodiment
[0013] Example 3. A method for reducing tin tetrachloride, which uses electricity as a reducing agent; its specific steps are as follows: add it to an electrolytic cell equipped with a tail gas treatment system, stirring, a nickel electrode as the cathode, and a metal electrode with iridium, tantalum, and titanium as the anode The dilute hydrochloric acid solution of tin tetrachloride produced by the reduction of diazonium salt with stannous chloride, stir and energize to 18A; slowly increase the temperature and react at 75°C; after detecting that there is no tetravalent tin in the solution, the reaction ends, that is Obtain a dilute hydrochloric acid solution of stannous chloride.
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