Low-temperature slag-free zinc bonderite as well as preparation method and applications thereof
A phosphating agent and zinc-based technology, which is applied in the coating process of metal materials, etc., can solve the problems of high energy consumption, waste of resources, and high labor intensity, and achieve low energy consumption, lower unit cost, and fine phosphating film Effect
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Embodiment 1
[0049] Preparation:
[0050] According to the preparation of 1000kg low-temperature slag-free zinc-based phosphating agent, 285kg of nitric acid, 105kg of phosphoric acid, 96kg of zinc oxide, 16kg of soda ash, 2.2kg of citric acid, 1.2kg of sodium fluoride, 1.0kg of sodium nitrite and 50kg of complexing agent, the balance for water.
[0051] 50kg of complexing agent contains 5kg of EDTA, 1.5kg of citric acid, 3kg of tartaric acid, 0.5kg of sodium tungstate, and the balance is water.
[0052] The preparation process is as follows:
[0053] First, zinc oxide, soda ash, citric acid, sodium fluoride, and sodium nitrite are mixed with water to make a paste, and then nitric acid, phosphoric acid, zinc oxide paste, soda ash paste, citric acid paste, fluorine Sodium chloride paste, sodium nitrite paste and complexing agent are put into the reaction kettle, the reaction is completed after 2 hours, and water is added to 1000 parts to obtain a low-temperature slag-free zinc-based phosp...
Embodiment 2
[0056] Preparation:
[0057] According to the preparation of 1000kg low-temperature slag-free zinc-based phosphating agent, 280kg of nitric acid, 100kg of phosphoric acid, 93kg of zinc oxide, 15kg of soda ash, 2.0kg of citric acid, 1.0kg of sodium fluoride, 1.0kg of sodium nitrite and 48kg of complexing agent, the balance for water.
[0058] 48kg of complexing agent contains 4.5kg of EDTA, 0.8kg of citric acid, 3.5kg of tartaric acid, 0.7kg of sodium tungstate, and the balance is water.
[0059] The preparation process is as follows:
[0060] First, zinc oxide, soda ash, citric acid, sodium fluoride, and sodium nitrite are mixed with water to make a paste, and then nitric acid, phosphoric acid, zinc oxide paste, soda ash paste, citric acid paste, fluorine Sodium chloride paste, sodium nitrite paste and complexing agent are put into the reaction kettle, the reaction is completed after 2 hours, and water is added to 1000 parts to obtain a low-temperature slag-free zinc-based p...
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