Flame-retardant polysulfide sealant and preparation method thereof
A polysulfide sealant, flame-retardant technology, applied in chemical instruments and methods, adhesives, other chemical processes, etc., can solve the problem of poor flame retardancy of two-component polysulfide sealant, achieve good flame-retardant effect, add Small amount, avoiding the effect of flammability
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[0036] The preparation method of the above-mentioned flame-retardant polysulfide sealant is as follows:
[0037] Dry the filler and flame retardant at 60-80°C for 1 hour; put the dried filler, flame retardant, liquid silane-modified polysulfide rubber, tackifier, and plasticizer into the kneader and mix evenly. The paste is ground by a colloid mill, and then dehydrated in a reactor under vacuum to obtain the one-component flame-retardant polysulfide sealant.
[0038] In the polysulfide sealant in the embodiment of the present invention, the flame retardant formed by compounding flame-retardant graphite and antimony trioxide is used as a flame-retardant system, and the amount of addition is small, so that the density of the sealant is small and the consumption per unit volume is small; The sealant has good flame retardant effect, the oxygen index is greater than 34%, and meets the FV-0 standard, and the sealant does not contain volatile components, and will not corrode glass, s...
Embodiment 1
[0041] This embodiment provides a flame-retardant polysulfide sealant, which is a single-component polysulfide sealant. The amount of each raw material (by mass percentage) of the sealant is:
[0042]
[0043] The preparation method of the above-mentioned sealant is as follows: dry flame-retardant graphite, antimony trioxide, barium titanate, and calcium carbonate at 60-80°C for 1 hour; dry liquid silane-modified polysulfide rubber, dibutyl phthalate , rosin resin, dried filler and flame retardant are put into a kneader and mixed evenly. The mixed paste is ground by a colloid mill, and then dehydrated in a reactor under vacuum to obtain a one-component flame-retardant polymer. Sulfur sealant.
Embodiment 2
[0045] This embodiment provides a flame-retardant polysulfide sealant, which is a single-component polysulfide sealant. The amount of each raw material (by mass percentage) of the sealant is:
[0046]
[0047] The preparation method of above-mentioned sealant is as follows:
[0048] Dry flame-retardant graphite, antimony trioxide, kaolin, and carbon black at 60-80°C for one hour; dry liquid silane-modified polysulfide rubber, dioctyl phthalate, terpene resin, and dried filler 1. The flame retardant is put into a kneader and mixed evenly. The mixed paste is ground by a colloid mill, and then dehydrated in a reactor under vacuum to obtain a one-component flame-retardant polysulfide sealant.
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