Method for preparing fiber-reinforced epoxy resin-based composite material super-hydrophobic surface

A fiber-reinforced material and super-hydrophobic surface technology, which is applied in the field of super-hydrophobic surface material preparation, can solve the problems of unsuitable super-hydrophobic surface preparation, etc., and achieve good industrial application prospects, simple operation process, good self-cleaning and waterproof Effect

Active Publication Date: 2014-01-15
NAT UNIV OF DEFENSE TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The existing superhydrophobic surface preparation methods include electrospinning method, sol-gel method, plasma fluorination method, electrochemical method, etc., but these methods are not suitable for the preparation of superhydrophobic surface of fiber-reinforced epoxy resin matrix composites.

Method used

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  • Method for preparing fiber-reinforced epoxy resin-based composite material super-hydrophobic surface
  • Method for preparing fiber-reinforced epoxy resin-based composite material super-hydrophobic surface
  • Method for preparing fiber-reinforced epoxy resin-based composite material super-hydrophobic surface

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Experimental program
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Effect test

Embodiment 1

[0026] A kind of preparation method of superhydrophobic surface of fiber-reinforced epoxy resin matrix composite material of the present invention, comprises the following steps:

[0027] 1. Prepare ingredients

[0028] 1.1 Prepare fiber reinforced material: take carbon fiber cloth and cut it into 10cm×15cm, set aside;

[0029] 1.2 Prepare inorganic powder calcium carbonate (or zinc oxide);

[0030] 1.3 Prepare E-51 epoxy resin glue and diethylenetriamine for use.

[0031] 2. Prepare the resin system

[0032] 2.1 Mix and dilute 8g of calcium carbonate and 2g of E-51 epoxy resin glue in 50ml of acetone, stir well and then add 0.2g of diethylenetriamine to form the outer coating resin system;

[0033] 2.2 Weigh 8g of E-51 epoxy resin glue and 0.8g of diethylenetriamine and mix well to form the middle layer resin system.

[0034] 3. Coating resin system

[0035] Take a molding mold, polish the mold and apply a release agent, and place the release paper in the mold; then appl...

Embodiment 2

[0042] A kind of preparation method of superhydrophobic surface of fiber-reinforced epoxy resin matrix composite material of the present invention, comprises the following steps:

[0043] 1. Prepare ingredients

[0044] 1.1 Prepare fiber reinforced material: take carbon fiber cloth and cut it into 15cm×15cm for use;

[0045] 1.2 Prepare inorganic powder calcium carbonate (or zinc oxide);

[0046] 1.3 Prepare E-51 epoxy resin glue and diethylenetriamine for use.

[0047] 2. Prepare the resin system

[0048] 2.1 Mix and dilute 7g of calcium carbonate and 3g of E-51 epoxy resin glue in 50ml of acetone, stir well and then add 0.3g of diethylenetriamine to form the outer coating resin system;

[0049] 2.2 Weigh 27g of E-51 epoxy resin glue and 2.7g of diethylenetriamine and mix well to form the middle layer resin system.

[0050] 3. Coating resin system

[0051] Take a molding mold, polish the mold and apply a release agent, and place the release paper in the mold; then apply th...

Embodiment 3

[0058] A kind of preparation method of superhydrophobic surface of fiber-reinforced epoxy resin matrix composite material of the present invention, comprises the following steps:

[0059] 1. Prepare ingredients

[0060] 1.1 Prepare fiber reinforced material: take glass fiber cloth and cut it into 20cm×20cm for use;

[0061] 1.2 Prepare metal oxide powder zinc oxide (or calcium carbonate);

[0062] 1.3 Prepare E-51 epoxy resin glue and diethylenetriamine for use.

[0063] 2. Prepare the resin system

[0064] 2.1 Mix and dilute 9g of calcium carbonate and 1g of E-51 epoxy resin glue in 80ml of acetone, stir well and then add 0.1g of diethylenetriamine to form the outer coating resin system;

[0065] 2.2 Weigh 49g of E-51 epoxy resin glue and 4.9g of diethylenetriamine and mix well to form the middle layer resin system.

[0066] 3. Coating resin system

[0067] Take a molding mold, polish the mold and apply a release agent, and place the release paper in the mold; then apply...

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Abstract

The invention discloses a method for preparing a superhydrophobic surface of a fiber-reinforced epoxy resin-based composite material. Proportionally mixed to form the outer coating resin system; another epoxy resin and curing agent were weighed and mixed to form the middle layer resin system; the outer coating resin system was first coated in a molding mold, and the first layer of fiber was laid Reinforcement material; then coat the intermediate layer resin system on it, and lay the second layer of fiber reinforcement material; then repeat the intermediate layer resin system on it, and so on, to obtain the composite material preform; finally after curing , acid leaching, taking out, and drying to obtain the superhydrophobic surface of the fiber-reinforced epoxy resin-based composite material. The preparation method of the invention has the advantages of simple operation process, good controllability, good reproducibility, low cost, environmental protection and safety, excellent product quality and the like.

Description

technical field [0001] The invention relates to a preparation method of a superhydrophobic surface material, in particular to a preparation method of a superhydrophobic surface of an epoxy resin-based composite material. Background technique [0002] Fiber-reinforced epoxy resin-based composites have attracted extensive attention due to their designability, high specific strength, and light weight. They have very important applications in various fields such as wind turbine blades, large aircraft, ships, and automobiles. However, the surface of the current commercial fiber-reinforced epoxy resin-based composites is not self-cleaning, and it is easy to accumulate dust after long-term use outdoors, which affects the appearance. When sewage drops (or splashes) on the surface of fiber-reinforced epoxy resin-based composites When it is not wiped off in time, obvious pollution marks will often be left on the surface. In addition, many epoxy resin-based composite materials have cer...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B32B37/15B32B37/06B32B37/10
Inventor 袁志庆肖加余王春齐曾竟成刘钧邢素丽张鉴炜朱宝军江大志
Owner NAT UNIV OF DEFENSE TECH
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