Preparation method of composite ordered porous nanometer titanium dioxide (TiO2) film
A nano-titanium dioxide and thin film technology, applied in the field of dye-sensitized solar cells, can solve problems such as electron-hole recombination, achieve the effects of large specific surface area, inhibit electron-hole recombination, and increase adsorption capacity
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[0024] Below in conjunction with example and accompanying drawing, the present invention is described in further detail.
[0025] Preparation of polystyrene microsphere emulsion and assembly of polystyrene microsphere colloidal crystal template: Pour styrene into a separatory funnel, wash it four times with 0.1M NaOH solution and secondary deionized water to remove inhibition Add 40mL of secondary deionized water and 0.0125g of sodium dodecylbenzenesulfonate into a 100mL four-necked flask, stir to dissolve, heat the water bath to 78°C, and then pass in nitrogen, then add 0.04g of NaHCO 3 and 10mL of washed styrene monomer; continue to heat and reflux and stir for 1 hour, and 0.1gK 2 S 2 o 8 Dissolve it in 10mL of secondary deionized water and drop it into a flask, control the temperature at (78±2)°C, heat to reflux and stir to react for 12 hours, then stop the reaction to obtain a polystyrene microsphere emulsion with a particle size of 450nm.
[0026] Using FTO conductive ...
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