Method for preparing Poria cocos granules by replacing part of auxiliary materials with ultrafine powder
A formula granule and superfine powder technology, which is applied to medical preparations with non-active ingredients, medical preparations containing active ingredients, and pharmaceutical formulas, etc. It can solve the problems of low extraction rate of Poria cocos decoction pieces, increased production costs, and large energy consumption. , to achieve better taste, increased hydrophilicity and good taste
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Embodiment 1
[0046] Take 98 kg of Poria cocos decoction pieces, add water to decoct twice, add 8 times the amount of water for the first time, decoct for 2 hours; add 7 times the amount of water for the second time, decoct for 1 hour, filter the liquid medicine, and concentrate in a vacuum (vacuum degree -0.05~-0.07MPa, 60~70°C) until the total amount of liquid medicine is 5L, pass through a 180-mesh sieve to obtain a concentrated solution of Poria cocos for future use;
[0047] Take 2 kg of Poria decoction pieces, crush them with a high-speed pulverizer, pass through an 80-mesh sieve, and pulverize them with an airflow pulverizer, adjust the frequency of the grading impeller to 35 Hz, collect ultrafine powder with a particle size of less than 500 mesh, add 5 L of water, and then add 0.8 kg of maltodextrin , heated and boiled for 20 minutes, then stood still for 30 minutes, stirred evenly, adjusted the speed of the colloid mill to 3000 rpm, adjusted the gap between the stator and rotor of t...
Embodiment 2
[0050] Take 98.5kg of Poria cocos decoction pieces, add water to decoct twice, add 9 times the amount of water for the first time, decoct for 1 hour; add 6 times the water for the second time, decoct for 1 hour, filter the liquid medicine, vacuum Concentrate (vacuum degree -0.05~-0.07MPa, 60~70°C) until the total amount of medicinal solution is 8L, pass through a 350-mesh sieve to obtain Poria cocos concentrate;
[0051] Take 1.5 kg of Poria cocos decoction pieces, pulverize them with a high-speed pulverizer, pass through a 100-mesh sieve, and pulverize them with an airflow pulverizer, adjust the frequency of the grading impeller to 30 Hz, collect ultrafine powder with a particle size of less than 500 mesh, add 8 L of Poria cocos concentrate, add β- Cyclodextrin 0.6kg, heat and boil for 30 minutes, then stand still for 30 minutes, stir evenly, control the temperature of the feed liquid at 65°C~75°C, adjust the speed of the colloid mill to 2500 rpm, and adjust the gap between th...
Embodiment 3
[0054] Take 97kg of Poria decoction pieces, add water to decoct twice, add 8 times the amount of water for the first time, decoct for 2 hours; add 7 times the amount of water for the second time, decoct for 1 hour, filter the liquid medicine, and concentrate in vacuo (vacuum degree -0.05~-0.07MPa, 60~70°C) until the total amount of liquid medicine is 5L, pass through a 180-mesh sieve, control the inlet air temperature at 160~170°C, the outlet air temperature at 85~95°C, and the negative pressure in the tower- 0.01~-0.05MPa, collect the spray-dried powder to obtain Poria cocos concentrated powder;
[0055] Take 3 kg of Poria decoction pieces, pulverize them with a high-speed pulverizer, pass through a 80-mesh sieve, pulverize with an airflow pulverizer, adjust the frequency of the grading impeller to 35 Hz, collect ultrafine powder with a particle size of less than 500 mesh, add 12 L of water, add 1 kg of maltodextrin, and heat Boil for 20 minutes, then stand still for 30 minut...
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