This application belongs to the field of nanophotocatalytic materials technology, and discloses a mesoporous TiO2 /
coumarin-doped
graphitic carbon nitride (CM-CN) composite photocatalyst, its preparation method, and its application. The invention first uses a
crystallization-driven single-colloidal
assembly method to prepare TiO2 particles with a uniform mesoporous structure. Then, dihydroxycoumarin is mixed with
urea using a thermal polycondensation method and calcined at high temperature to obtain CM-CN. Next, CM-CN and mesoporous TiO2 are self-assembled in a
solvent using a
solvent dispersion-promoting technique to obtain the mesoporous TiO2 / CM-CN composite photocatalyst. This mesoporous TiO2 / CM-CN composite photocatalyst possesses a hierarchical pore structure, high specific surface area, excellent hydrophilicity, and strong
interfacial bonding, achieving efficient transfer and separation of photogenerated carriers, and enabling the construction of a green, stable, and highly active photocatalytic
system. The material preparation process is simple, the
raw material cost is controllable, there is no secondary
pollution, and the photocatalytic performance is significant, showing good potential for large-scale production and widespread application.