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High strength rubber with radiation resistance and thermal aging resistance and preparation method thereof

A technology of heat aging resistance and radiation resistance, which is applied in the fields of new rubber and its preparation, high-strength rubber and its preparation, and can solve the problems of inability to improve radiation resistance, decline in rubber mechanical properties, and limited radiation resistance. Achieve good social and economic benefits, good mechanical properties, excellent radiation resistance and heat aging resistance

Active Publication Date: 2012-07-04
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But the rare earth oxides in this process are simply physical blending
The consequence of this is that when the amount added reaches a certain value, the radiation performance reaches a stable extreme value, so its radiation resistance is limited.
If you continue to add fillers, the radiation resistance cannot be improved, and at the same time, it will cause serious phase separation, resulting in a serious decline in the mechanical properties of the rubber.

Method used

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  • High strength rubber with radiation resistance and thermal aging resistance and preparation method thereof
  • High strength rubber with radiation resistance and thermal aging resistance and preparation method thereof
  • High strength rubber with radiation resistance and thermal aging resistance and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Take the following components in parts by weight (kg): 100 parts of nitrile rubber raw rubber (nitrile rubber raw rubber, its acrylonitrile mass fraction is 41%), 5 parts of rare earth salts (gadolinium chloride), 70 parts of strengthening agent (carbon black, N220 produced by American Cabot Company).

[0026] First, add the raw nitrile rubber, carbon black, and rare earth salts of the component amount to the mixer in sequence, and knead at room temperature for 30 minutes, then heat-treat the kneaded material at 190°C for 1 hour, and knead again. Evenly, the rubber base material with radiation resistance can be obtained, and the rubber product with radiation resistance can be obtained by molding and vulcanizing the base material.

Embodiment 2

[0028] The specific operation method is the same as that of Example 1, except that the component amount of gadolinium chloride is changed to 10 parts in the ratio of the rare earth salt component.

Embodiment 3

[0030] The specific operation method is the same as that of Example 1, except that the component amount of gadolinium chloride is changed to 15 parts in the proportion of rare earth salt components.

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Abstract

The invention discloses high strength rubber with both the radiation resistance and the thermal aging resistance, which comprises the following components in parts by weight: 100 parts of crude rubber, 1 to 50 parts of rare earth salt, 10 to 100 parts of reinforcing agent and 0 to 20 parts of other ingredients. The high strength rubber with both the radiation resistance and the thermal aging resistance of the invention has strong environmental adaptability, has tensile strength of over 16MPa and tearing strength of over 40KN / m after being irradiated under the condition of 300KGy, can be used for producing various rubber products with various radiation resistance properties, which comprise a rubber gasket, a seal part, a shock absorbing and buffering part, a spacer bush, a diaphragm and the like, can be widely applied to the environment with high energy radiation in various fields of aerospace, nuclear industry, electronic communication, chemical industry, medicine, watercraft and the like, and has good economic benefits and popularization value.

Description

technical field [0001] The invention relates to a novel rubber and a preparation process thereof, in particular to a high-strength rubber having both radiation resistance and heat aging resistance and a preparation method thereof, belonging to the technical field of rubber production. Background technique [0002] At present, my country's aerospace, atomic energy industry and military fields are developing rapidly. In these fields, a large number of rubber materials are used, such as: various sealing materials used in the supporting equipment of atomic reactors and aerospace equipment exposed to space radiation. pieces etc. Under normal circumstances, the existing rubber is exposed to high-energy radiation, which will cause a series of chemical changes such as chain scission or cross-linking reactions in the rubber macromolecules, and the structure and composition of the material will be destroyed, resulting in serious degradation and failure of the material. Recently, with ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L9/02C08K13/02C08K3/16C08K3/04C08K3/36C08K5/098C08K3/22
Inventor 冯圣玉韩建军卢海峰
Owner SHANDONG UNIV
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