Silicon carbide ceramic heat-exchanging board and manufacturing method thereof
A technology of silicon carbide ceramics and heat exchange plates, applied in the field of engineering ceramic materials, can solve the problems of lack of design, low yield and difficulty in forming
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[0102] The preparation method of heat exchange plate of the present invention comprises the steps:
[0103] (a) providing (85-95) parts by weight of silicon carbide powder, (0-15) parts by weight of sintering aid, and (0-2) parts by weight of binder for granulation to obtain powder;
[0104] (b) molding the powder in step (a) to obtain a silicon carbide green body;
[0105] (c) molding the silicon carbide green body to obtain a molded body, the molded body has a centrosymmetric structure, and the centrosymmetric structure includes a square or a circle; and the molded body is provided with a double-circuit heat exchange structure aisle;
[0106] (d) The molded body is subjected to subsequent steps to obtain the heat exchange plate.
[0107] granulation
[0108] In a preferred example, the sintering aid may include B 4 C-C, B-C, where C can be introduced as powder or produced by cracking organic matter. where B 4 The content of C or B is 0.2-2wt%, preferably 0.4-1.0wt%, ...
Embodiment 1
[0137] Mix 95wt% of silicon carbide powder, 1.0wt% of nano-carbon black and 0.4wt% of boron carbide powder in alcohol solution, add binder phenolic resin and mix in sand mill for 4 hours before spraying grain. The powder after spray granulation is dry-pressed and isostatically pressed into a square green body. The green body is processed into figure 1 Then heat treatment in a vacuum graphite resistance furnace, the temperature is 600 ° C for 4 hours, the heating rate is 1 ° C / min, the green body after heat treatment is sintered in a high temperature sintering furnace, 2150 ° C for 4 hours, Ar atmosphere, heating rate 2°C / min.
[0138] The parameters of the heat exchange plate after sintering are: the total thickness is 4mm, the depth of the heat exchange channel is 2mm, the width of the divider wall between the heat exchange channels is 2mm, the depth of the holes on the divider wall is 1.3mm, the width is 4mm, the spacing 15mm. The width of the dividing wall perpendicul...
Embodiment 2
[0141] Mix 95wt% of silicon carbide powder, 3.0wt% of nano-carbon black and 1.0wt% of amorphous boron powder in an aqueous solution, add binder phenolic resin and mix in a sand mill for 8 hours before spray granulation . The powder after spray granulation is dry-pressed and isostatically pressed into a round green body. The green body is processed into figure 2 Then heat treatment in a vacuum graphite resistance furnace, the temperature is 1200 ° C for 1 h, the heating rate is 5 ° C / min, the green body after heat treatment is sintered in a high temperature sintering furnace, 2250 ° C for 2 h, Ar atmosphere, heating rate 10°C / min.
[0142] The sintered furnace sample was tested to obtain a density of 98.6% T.D. and a thermal conductivity of 132W (m·K) at room temperature.
[0143] The parameters of the heat exchange plate after sintering are: the total thickness is 10mm, the depth of the heat exchange channel is 5mm, the width of the divider wall between the heat exchange...
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