Production process of wool protein compound viscose fiber
A technology of wool protein and viscose fiber, which is applied in the fields of fiber chemical characteristics, cellulose/protein conjugated artificial filament, and chemical post-treatment of cellulose/protein artificial filament. Protein sedimentation, poor fiber spinnability and other problems, to avoid the reduction of fiber strength and improve the effect of fiber strength
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Embodiment 1
[0037] A production process of wool protein composite viscose fiber, comprising the following process steps:
[0038] A. Preparation of wool protein spinning solution: take wool protein and sodium hydroxide, dissolve wool protein in aqueous sodium hydroxide solution, and completely dissolve wool protein solution in sodium hydroxide solution without precipitation and maintain pH value at 9 Accurately, the wool protein solution is obtained by filtration, and then hydrogen peroxide is added to the wool protein solution for initiation, and then the auxiliary agent PEG200 is added in a certain proportion to obtain the wool egg self-spinning solution;
[0039]B. Blending of wool protein liquid and viscose spinning solution: after defoaming the wool protein spinning solution and the composite cellulose viscose spinning solution respectively, carry out static mixing according to a certain proportion and degas again to obtain viscose;
[0040] The above-mentioned composite cellulose sp...
Embodiment 2
[0055] A production process of wool protein composite viscose fiber, comprising the following process steps:
[0056] A. Preparation of wool protein spinning solution: take wool protein and sodium hydroxide, dissolve wool protein in aqueous sodium hydroxide solution, and completely dissolve wool protein solution in sodium hydroxide solution without precipitation and keep the pH value at 14. Accurately, the wool protein solution is obtained by filtration, and then hydrogen peroxide is added to the wool protein solution for initiation, and then the auxiliary agent PEG200 is added in a certain proportion to obtain the wool egg self-spinning solution;
[0057] B. Blending of wool protein liquid and viscose spinning solution: after defoaming the wool protein spinning solution and the composite cellulose viscose spinning solution respectively, carry out static mixing according to a certain proportion and degas again to obtain viscose;
[0058] The above-mentioned composite cellulose...
Embodiment 3
[0073] A production process of wool protein composite viscose fiber, comprising the following process steps:
[0074] A. Preparation of wool protein spinning solution: take wool protein and sodium hydroxide, dissolve wool protein in aqueous sodium hydroxide solution, completely dissolve wool protein solution in sodium hydroxide solution without precipitation and maintain pH value at 11.5 Accurately, the wool protein solution is obtained by filtration, and then hydrogen peroxide is added to the wool protein solution for initiation, and then the auxiliary agent PEG200 is added in a certain proportion to obtain the wool egg self-spinning solution;
[0075] B. Blending of wool protein liquid and viscose spinning solution: after defoaming the wool protein spinning solution and the composite cellulose viscose spinning solution respectively, carry out static mixing according to a certain proportion and degas again to obtain viscose;
[0076] The above-mentioned composite cellulose sp...
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