Production process of wool protein compound viscose fiber

A technology of wool protein and viscose fiber, which is applied in the fields of fiber chemical characteristics, cellulose/protein conjugated artificial filament, and chemical post-treatment of cellulose/protein artificial filament. Protein sedimentation, poor fiber spinnability and other problems, to avoid the reduction of fiber strength and improve the effect of fiber strength

Active Publication Date: 2012-07-11
CHENGDU GRACE FIBER +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This substance will still remain on the fiber after subsequent washing, which is impossible under the current environmental protection pressure of actual production, and the heavy metals and toxic substances in the finished product exceed the standard
[0005] In addition, due to the use of a variety of animal proteins, the source is relatively complicated, and the properties (protein content, solution viscosity, etc.) and stability of the protein solution are very low
[0006] Since the above-mentioned patent adopts discontinuous production, there will often be a certain stock of protein liquid, and the existence of tyrosine crystal substances in the protein liquid will lead to protein sedimentation and flocculation, making the spinnability of subsequent fibers extremely poor, and easy to block and spray Filament head and filter element, produce a large number of coarse fibers and doubling

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] A production process of wool protein composite viscose fiber, comprising the following process steps:

[0038] A. Preparation of wool protein spinning solution: take wool protein and sodium hydroxide, dissolve wool protein in aqueous sodium hydroxide solution, and completely dissolve wool protein solution in sodium hydroxide solution without precipitation and maintain pH value at 9 Accurately, the wool protein solution is obtained by filtration, and then hydrogen peroxide is added to the wool protein solution for initiation, and then the auxiliary agent PEG200 is added in a certain proportion to obtain the wool egg self-spinning solution;

[0039]B. Blending of wool protein liquid and viscose spinning solution: after defoaming the wool protein spinning solution and the composite cellulose viscose spinning solution respectively, carry out static mixing according to a certain proportion and degas again to obtain viscose;

[0040] The above-mentioned composite cellulose sp...

Embodiment 2

[0055] A production process of wool protein composite viscose fiber, comprising the following process steps:

[0056] A. Preparation of wool protein spinning solution: take wool protein and sodium hydroxide, dissolve wool protein in aqueous sodium hydroxide solution, and completely dissolve wool protein solution in sodium hydroxide solution without precipitation and keep the pH value at 14. Accurately, the wool protein solution is obtained by filtration, and then hydrogen peroxide is added to the wool protein solution for initiation, and then the auxiliary agent PEG200 is added in a certain proportion to obtain the wool egg self-spinning solution;

[0057] B. Blending of wool protein liquid and viscose spinning solution: after defoaming the wool protein spinning solution and the composite cellulose viscose spinning solution respectively, carry out static mixing according to a certain proportion and degas again to obtain viscose;

[0058] The above-mentioned composite cellulose...

Embodiment 3

[0073] A production process of wool protein composite viscose fiber, comprising the following process steps:

[0074] A. Preparation of wool protein spinning solution: take wool protein and sodium hydroxide, dissolve wool protein in aqueous sodium hydroxide solution, completely dissolve wool protein solution in sodium hydroxide solution without precipitation and maintain pH value at 11.5 Accurately, the wool protein solution is obtained by filtration, and then hydrogen peroxide is added to the wool protein solution for initiation, and then the auxiliary agent PEG200 is added in a certain proportion to obtain the wool egg self-spinning solution;

[0075] B. Blending of wool protein liquid and viscose spinning solution: after defoaming the wool protein spinning solution and the composite cellulose viscose spinning solution respectively, carry out static mixing according to a certain proportion and degas again to obtain viscose;

[0076] The above-mentioned composite cellulose sp...

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PUM

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Abstract

The invention provides a production process of wool protein compound viscose fiber, which belongs to the technical field of viscose fiber. The process comprises the steps of preparing a wool protein spinning solution, blending the wool protein spinning solution with a viscose spinning solution, spinning, solidifying and curing and performing aftertreatment to obtain the wool protein compound viscose fiber. In the invention, the addition of toxic substances is avoided, the obtained finished product is more suitable for manufacturing the textile products with high safety, such as intimate apparels and the like, and shows the advantages in environmental friendliness.

Description

technical field [0001] The invention relates to a production process of viscose fiber, in particular to a production process of wool protein composite viscose fiber, which belongs to the field of viscose fiber. Background technique [0002] Wool is a natural protein fiber resource that has been used by humans for a long time. According to the latest statistics released by the International Wool Textile Organization, in the past 8 years, the world's total wool production has dropped by 160 million kg net wool, while the production of wool for clothing has dropped by 18%. In 2009-2010, wool production declined again, which shows that wool resources are facing a shortage. Wool is one of the largest imports of animal products in my country. At present, the import volume has accounted for 2 / 3 of the domestic wool production, and has become one of the largest wool importing countries in the world. However, domestic wool is at a disadvantage compared with imported wool in terms of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F8/02D01F1/10D01F11/02D01D5/06D01D5/16
Inventor 龙国强涂平杜咏林赵建明
Owner CHENGDU GRACE FIBER
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