Inorganic electromagnetic-wave absorbing material and preparation method thereof
A technology for absorbing materials and electromagnetic waves, applied in chemical instruments and methods, and other chemical processes, can solve problems such as the influence of wave-absorbing performance, easy changes in shape, thickness, and size, and the inability to use wave-absorbing materials, so as to overcome temperature resistance Poor weather resistance, good oxidation resistance and low cost
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Embodiment 1
[0033] In this example, 560g carbonyl iron powder and 440g glass powder are mixed in a rolling mill. The average particle size of the carbonyl iron powder is 1 micron, the average particle size of the glass powder is 6 microns, the softening point of the glass powder is 500°C, and the ball weight The ratio is 5:1, the ball milling time is 12 hours, and the speed is 80r / min. Add 136 g of CMC with a concentration of 4 wt% to the mixed powder and mix, and pass through a 60-mesh sieve to obtain granulated powder. According to the product size, the granulated powder is weighed, put into a mold, and formed on a press to obtain a green body. The formed green body is fired in an atmosphere furnace using a ceramic sintering process, the atmosphere is nitrogen, the firing temperature is 550°C, and the firing temperature is kept for 40 minutes.
[0034] The strength of the carbonyl iron / glass composite absorbing material prepared by the invention is 52MPa, which meets the requirements of l...
Embodiment 2
[0036] In this example, 50g carbon nanotubes and 950g glass powder are mixed in a stirring mill. The average size of carbon nanotubes is 0.01 micron, the average particle size of glass powder is 0.1 micron, the softening point of glass powder is 650℃, and the mixing time is 2 hours, the speed is 450r / min. Add 53 g of PVB with a concentration of 10 wt% to the mixed powder and mix, and pass through a 100-mesh sieve to obtain granulated powder. According to the product size, the granulated powder is weighed, put into a mold, and formed on a press to obtain a green body. The formed green body is fired in an atmosphere furnace using a ceramic sintering process, the atmosphere is high-purity argon, the firing temperature is 730°C, and the firing temperature is kept for 10 minutes.
[0037] The strength of the carbon nanotube / glass composite absorbing material prepared by the invention is 42MPa, which meets the requirements of later mechanical processing; Figure 4 It can be seen that ...
Embodiment 3
[0039] In this example, 300g of silicon carbide and 700g of glass powder are mixed in a planetary mill. The average particle size of silicon carbide is 10 microns, the average particle size of glass powder is 2 microns, the softening point of glass powder is 750°C, and the ball-to-material weight ratio is 2:1, rotation speed is 200r / min, ball milling time is 6 hours. To the mixed powder, 87g of PVA with a concentration of 5 wt% was added and mixed, and then passed through a 40-mesh sieve to obtain granulated powder. According to the product size, the granulated powder is weighed, put into a mold, and formed on a press to obtain a green body. The formed green body is fired in a silicon carbide rod high-temperature furnace using a ceramic sintering process, the atmosphere is air, the firing temperature is 850 DEG C, and the firing temperature is kept for 20 minutes.
[0040] The strength of the silicon carbide / glass composite wave absorbing material prepared by the invention is 45...
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Abstract
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Application Information
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