Silicon wafer chemical-mechanical polishing composition with high dilution ratio and high stability
A polishing composition, high stability technology, applied in the direction of polishing composition containing abrasives, etc., can solve the problems of not meeting the requirements of planarization of integrated circuits, high cost of polishing composition, increase of polishing damage layer, etc., to achieve polishing Effect of rate acceleration, improvement of pH buffering performance, and reduction of surface roughness
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Embodiment 1
[0030] Prepare 100g of the chemical mechanical polishing composition for silicon wafers, the preparation process is as follows: add 2.0g 10wt% tetramethylammonium hydroxide aqueous solution to 93.23g 60-80nm 41wt% silica sol; 1g ethanolamine; 0.3g diethylenetri Amine; 0.1g AMP-95, 0.01g glycine, 0.01g TX-10, 0.35g potassium carbonate, 3g pH=11 buffer system. It is prepared by mixing and stirring, and the pH of the prepared polishing composition is 11.23.
[0031] Use and result analysis: When using the polishing composition, first dilute the prepared polishing composition with deionized water at a ratio of 1:30, perform polishing experiments on silicon wafers that pass the inspection, and paste the polished silicon wafers On the polishing disc of Lanzhou Ruide large-scale single-sided polishing machine, fix the polishing disc with silicon wafer on the polishing head of the machine, control the polishing pressure at about 0.16MPa, control the speed of the upper polishing disc t...
Embodiment 2
[0033] Prepare 100g of silicon wafer chemical mechanical polishing composition, the preparation process is as follows: add 0.05g tetramethylammonium hydroxide, 0.04g hydroxyethyl ethylenediamine, 0.01g AMP to 98.84g 60-80nm 41wt% silica sol -95 is prepared by mixing and stirring 0.8g trisodium nitrilotriacetate, 0.1g AEO-9, 0.01g sodium bicarbonate, and 0.15g buffer system with pH=12, and the pH of the prepared polishing composition is 11.42.
[0034] Use and result analysis: When using the polishing composition, first dilute the prepared polishing composition with deionized water at a ratio of 1:40, perform polishing experiments on silicon wafers that pass the inspection, and paste the polished silicon wafers On the polishing disc of Lanzhou Ruide large-scale single-sided polishing machine, fix the polishing disc with silicon wafer on the polishing head of the machine, control the polishing pressure at about 0.16MPa, control the speed of the upper polishing disc to 60rpm, and ...
Embodiment 3
[0036] Prepare 100g of silicon wafer chemical mechanical polishing composition, the preparation process is as follows: add 10g 5wt% isopropanolamine aqueous solution to 85.74g 60-80nm 41wt% silica sol; 1g ethanolamine; 1.3g diethylenetriamine; 0.2g AMP-95 is prepared by mixing and stirring 0.15g glycine, 1g TX-10, 0.6g dipotassium hydrogen phosphate, and 0.01g pH=12 buffer system, and the pH of the prepared polishing composition is between 11.15.
[0037] Use and result analysis: When using the polishing composition, first dilute the prepared polishing composition and deionized water at a ratio of 1:45, perform polishing experiments on silicon wafers that pass the inspection, and paste the polished silicon wafers On the polishing disc of Lanzhou Ruide large-scale single-sided polishing machine, fix the polishing disc with silicon wafer on the polishing head of the machine, control the polishing pressure at about 1.8kPa, control the speed of the upper polishing disc to 60rpm, an...
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