Degradable PBT/PLA (Polybutylece Terephthalate/Poly Lactic Acid) alloy and preparation method thereof
An alloy, polylactic acid technology, applied in the field of degradable PBT/PLA alloy and its preparation, can solve the problems of limited use, poor toughness of polylactic acid, low heat distortion temperature, etc., to solve the problem of recycling, improve compatibility, Heat resistance improvement effect
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[0049] The degradable PBT / PLA alloy of the embodiment of the present invention can adopt same preparation method, comprises the following steps:
[0050] (1) Pretreatment of raw materials;
[0051] (2) Take each component according to the following weight percentages:
[0052]
[0053] (3) Mix all the raw materials taken by weighing;
[0054] (4) Add the mixed raw materials into a parallel twin-screw extruder, melt and extrude, and granulate.
[0055] Twin-screw machines are generally divided into the following parts: feeding system, gearbox, main motor, screw, barrel, heating system, vacuum system, cooling system, interlock control system, and electrical control system. Among them, in the temperature control section of the heating system, it is divided into the feeding area, the first area, the second area, the third area, and the fourth area.
[0056] Among them, the process conditions of the melting stage of the parallel twin-screw extruder in the embodiment of the pres...
Embodiment 1
[0058] (1) Pretreatment of raw materials: PBT and PLA were dried separately, the drying temperature of PBT was 120°C for 4 hours; the drying temperature of PLA was 60°C for 4 hours. The remaining materials were dried at 80°C for 6 hours;
[0059] (2) Weigh PBT 73.5kg, PLA 20kg, EMA-GMA 4kg, antioxidant 10100.2kg, antioxidant 1680.2kg, lubricant TAF 0.6kg, transesterification accelerator tetrabutyl titanate 0.5kg, nucleating agent p-tert-butylcalix[8]arene 1kg;
[0060] (3) All the raw materials weighed were mixed in a high-speed mixer for 20 minutes;
[0061] (4) Add the uniformly mixed material into the hopper of the twin-screw extruder, melt, blend and extrude through the twin-screw extruder, water-cool, air-dry, pelletize, and finally bag the finished product of PBT / PLA alloy. Wherein, the screw speed is 200r / min.
[0062] The above-mentioned PBT / PLA alloy was injected into a standard sample, and the test performance is shown in Table 1.
Embodiment 2
[0064] (1) Pretreatment of raw materials: PBT and PLA were dried separately, the drying temperature of PBT was 120°C for 4 hours; the drying temperature of PLA was 60°C for 4 hours. The remaining materials were dried at 80°C for 6 hours;
[0065] (2) Weigh PBT 60kg, PLA 30kg, EMA-GMA 4kg, antioxidant 10760.2kg, antioxidant 1680.2kg, lubricant TAF 0.6kg, PETS 0.4kg, transesterification accelerator tetrabutyl titanate 0.5kg, Nucleating agent p-tert-butylcalix[8]arene 0.5kg;
[0066] (3) All the raw materials weighed were mixed in a high-speed mixer for 20 minutes;
[0067] (4) Add the uniformly mixed material into the hopper of the twin-screw extruder, melt, blend and extrude through the twin-screw extruder, water-cool, air-dry, pelletize, and finally bag the finished product of PBT / PLA alloy. Wherein, the screw speed is 200r / min.
[0068] The above-mentioned PBT / PLA alloy was injected into a standard sample, and the test performance is shown in Table 1.
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