Method for preparing ordered mesoporous titanium dioxide photocatalyst
A technology of mesoporous titanium dioxide and photocatalyst, applied in titanium dioxide, titanium oxide/hydroxide, physical/chemical process catalyst, etc., can solve the problem of poor mesoporous order, low photocatalytic activity, and small specific surface of mesoporous titanium dioxide, etc. problem, to achieve the effect of low cost, simple preparation process and improved photocatalytic activity
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specific Embodiment approach 1
[0015] Specific embodiment one: the preparation method of a kind of ordered mesoporous titanium dioxide photocatalyst in this embodiment is carried out according to the following steps:
[0016] 1. Surfactant functionalization: Weigh the surfactant, solvent and strong oxidant, wherein the mass ratio of surfactant to solvent is 0.01-0.25:1, and the mass ratio of strong oxidant to surfactant is 0.05-0.2:1 Dissolving the surfactant in a solvent, then adding a strong oxidizing agent, stirring for 1 to 48 hours at a temperature of 20 to 25° C. and a stirring speed of 100 to 300 r / min to obtain a surfactant solution;
[0017] 2. Preparation of titanium sol: Weigh titanium source and solvent according to the mass ratio of titanium source and solvent of 0.025 to 0.2:1, and dissolve the titanium source in the solvent to obtain a titanium solution, and then use the surfactant obtained in step one The solution is added to the titanium solution, and stirred for 0.5 to 24 hours to obtain a...
specific Embodiment approach 2
[0021] Specific embodiment 2: The difference between this embodiment and specific embodiment 1 is that the surfactant in step 1 is polyethylene oxide-polypropylene oxide-polyethylene oxide triblock copolymer P123, F127, twelve Sodium Alkyl Sulfate, Cetyltrimethylammonium Bromide, Acrylonitrile-Butadiene-Styrene Copolymer, Polyetherimide, Polyvinylpyrrolidone, Lauryl Polyethylene Glycol Ether, Polyethylene One or both of diol and triethanolamine are mixed in any proportion. Others are the same as in the first embodiment.
specific Embodiment approach 3
[0022] Specific embodiment 3: The difference between this embodiment and specific embodiment 1 or 2 is that the solvent in step 1 is deionized water, ethanol, isopropanol and n-butanol or mixed in any proportion. Others are the same as in the first or second embodiment.
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