Hydroxysulfobetaine amphoteric surfactant for flooding and preparation method of hydroxysulfobetaine amphoteric surfactant
A technology of sulfobetaine and surfactants, which is applied in the field of hydroxysulfobetaine amphoteric surfactants for oil displacement and its preparation, can solve the problems of poor resistance to salt and other problems, and achieve non-toxic, harmless and non-toxic products. Good thermal stability, good high temperature and salt resistance
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Embodiment 1
[0042] One, 296g methyl oleate, 117g benzene, and 1g methanesulfonic acid are used as catalysts, put into the reaction kettle, and feed N 2 After 30 minutes, react at 80°C for 10 hours, distill off unreacted aromatic hydrocarbons under reduced pressure, and recrystallize three times with absolute ethanol to obtain methyl aryl oleate with a yield of 91.3%.
[0043] 2. Put 250g methyl aryl oleate and 2.5g catalyst palladium carbon into the reactor, first use N 2 Replacement, then use H 2 After replacement, stir and heat up, the pressure is 0.1MPa, and the stirring speed is 500r / min. After the temperature reaches 230°C, raise the system pressure to 1.1MPa, start timing, take samples at regular intervals to measure the iodine value, until the iodine value no longer drops, cool down and depressurize the material, and the yield is 97.3%.
[0044]3. Weigh aryl oleyl alcohol and epichlorohydrin, 134g of 30% sodium hydroxide solution, and 1g of tetrabutylammonium bromide in a molar ...
Embodiment 2
[0048] One, with 296g methyl oleate, 158g mixed xylenes, 1g methanesulfonic acid as catalyst, put into reactor, pass into N 2 After 30 minutes, react at 80°C for 10 hours, distill off unreacted aromatic hydrocarbons under reduced pressure, and recrystallize three times with absolute ethanol to obtain methyl aryl oleate with a yield of 92.5%.
[0049] 2. Put 250g methyl aryl oleate and 2.5g catalyst into the reactor, first use N 2 Replacement, then use H 2 After replacement, stir and heat up, the pressure is 0.1MPa, and the stirring speed is 500r / min. After the temperature reaches 230°C, raise the system pressure to 1.1MPa, start timing, take samples at regular intervals to measure the iodine value, until the iodine value no longer drops, cool down and depressurize, and discharge, with a yield of 98.1%.
[0050] 3. Weigh aryl oleyl alcohol and epichlorohydrin, 134g of 30% sodium hydroxide solution, and 1g of tetrabutylammonium bromide in a molar ratio of 1:1, and place them ...
Embodiment 3
[0054] One, 296g methyl oleate, 138g toluene, 1g methanesulfonic acid are catalysts, put into reactor, pass into N 2 After 30 minutes, react at 80°C for 10 hours, distill off unreacted aromatic hydrocarbons under reduced pressure, and recrystallize three times with absolute ethanol to obtain methyl aryl oleate.
[0055] 2. Put 500g methyl aryl oleate and 2.5g catalyst into the reaction kettle, first use N 2 Replacement, then use H 2 After replacement, stir and heat up, the pressure is 0.1MPa, and the stirring speed is 500r / min. After the temperature reaches 230°C, raise the system pressure to 1.1MPa, start timing, take samples at regular intervals to measure the iodine value, until the iodine value no longer drops, then cool down and decompress and discharge.
[0056] 3. Weigh aryl oleyl alcohol and epichlorohydrin, 134g of 30% sodium hydroxide solution, and 1g of tetrabutylammonium bromide in a molar ratio of 1:1, and place them in a four-necked bottle equipped with an ele...
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